DOI: 10.1557/jmr.2005.0194. Preparation of Colloidal Bismuth Particles in Polyols

Preparation of Colloidal Bismuth Particles in Polyols

10.1557/jmr.2005.0194

Crossref journal-article

Springer Science and Business Media LLC

Journal of Materials Research (297)

Abstract

Nano- and micrometer size spherical bismuth particles were prepared by reducing bismuth salts in simple and mixed polyols at elevated temperatures. In general, the conversion to metallic bismuth was preceded by the formation, at intermediate temperatures, of bismuth-polyol compounds. By changing the type of bismuth salt, the composition of the polyol mixture, and the temperature of the process, these precursors were successfully converted into spherical bismuth particles. It was found that the reduction process proceeds only if the temperature of the polyol exceeds the values at which the intermediate bismuth-polyol are stable, which was determined to be around 220 °C.

Bibliography

Goia, C., MatijeviÄ, E., & Goia, D. V. (2005). Preparation of Colloidal Bismuth Particles in Polyols. Journal of Materials Research, 20(6), 1507â1514.

Authors 3

Corina Goia (first)
Egon Matijević (additional)
Dan V. Goia (additional)

References 25 Referenced 33

10.1021/ja00842a044 / J. Am. Chem. Soc. / Electroorganic chemistry. XXII. Novel anodic cleavage of glycols to carbonyl compounds. by Matsumura (1975)
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10.1103/PhysRevLett.82.3328 / Phys. Rev. Lett. / Large magnetoresistance and finite size effects in electrodeposited single crystal bismuth thin films. by Wang (1999)
10.1007/BF01132413
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{'key': 'S0884291400088038_ref025', 'first-page': '4', 'article-title': 'Conversion of uniform colloidal Cu2O spheres to copper in polyols.', 'volume': '18', 'author': 'Goia', 'year': '2003', 'journal-title': 'J. Mater. Res.'} / J. Mater. Res. / Conversion of uniform colloidal Cu2O spheres to copper in polyols. by Goia (2003)
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10.1023/A:1004895605613
10.1021/ja001118i

Dates

Type	When
Created	20 years, 2 months ago (June 3, 2005, 9:30 a.m.)
Deposited	4 years, 5 months ago (Feb. 24, 2021, 3:19 p.m.)
Indexed	1 year, 2 months ago (June 10, 2024, 12:37 p.m.)
Issued	20 years, 2 months ago (June 1, 2005)
Published	20 years, 2 months ago (June 1, 2005)
Published Online	20 years, 2 months ago (June 1, 2005)

Funders 0

None

BibTeX

@article{Goia_2005, title={Preparation of Colloidal Bismuth Particles in Polyols}, volume={20}, ISSN={2044-5326}, url={http://dx.doi.org/10.1557/jmr.2005.0194}, DOI={10.1557/jmr.2005.0194}, number={6}, journal={Journal of Materials Research}, publisher={Springer Science and Business Media LLC}, author={Goia, Corina and Matijević, Egon and Goia, Dan V.}, year={2005}, month=jun, pages={1507–1514} }

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