DOI: 10.1557/jmr.2002.0081. Preparation of Fine-grained BaTiO<sub>3</sub>Ceramics by Spark Plasma Sintering

Preparation of Fine-grained BaTiO3Ceramics by Spark Plasma Sintering

10.1557/jmr.2002.0081

Crossref journal-article

Springer Science and Business Media LLC

Journal of Materials Research (297)

Abstract

Dense BaTiO3ceramics consisting of fine grains were prepared using fine powder (average grain size of 0.06 μm; BT006) as a starting material and the spark plasma sintering (SPS) method. The powder was densified to >95% of theoretical x-ray density by the SPS process, and the average grain size of the resulting ceramics was <0.5 μm; the particle size of the initial powder significantly affects the grain size of the resulting SPS pellets. Fixed-frequency (100 kHz), room-temperature permittivity measurements of the BT006-SPS ceramics showed relatively low values (3000–3500) compared with those (typically 5000) for SPS ceramics consisting of larger grains (approximately 1 μm). Lower permittivity was attributed to poor development of ferroelectric domains in the ceramics, which originated from incomplete development of the tetragonal structure as well as the presence of a local orthorhombic structure.

Bibliography

Takeuchi, T., Capiglia, C., Balakrishnan, N., Takeda, Y., & Kageyama, H. (2002). Preparation of Fine-grained BaTiO3Ceramics by Spark Plasma Sintering. Journal of Materials Research, 17(3), 575â581.

Authors 5

Tomonari Takeuchi (first)
Claudio Capiglia (additional)
Nalini Balakrishnan (additional)
Yasuo Takeda (additional)
Hiroyuki Kageyama (additional)

References 32 Referenced 61

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Dates

Type	When
Created	17 years, 6 months ago (March 5, 2008, 9:41 p.m.)
Deposited	1 year, 6 months ago (Feb. 23, 2024, 1:53 a.m.)
Indexed	1 week, 1 day ago (Aug. 29, 2025, 6:20 a.m.)
Issued	23 years, 6 months ago (March 1, 2002)
Published	23 years, 6 months ago (March 1, 2002)
Published Online	14 years, 7 months ago (Jan. 31, 2011)
Published Print	23 years, 6 months ago (March 1, 2002)

Funders 0

None

BibTeX

@article{Takeuchi_2002, title={Preparation of Fine-grained BaTiO3Ceramics by Spark Plasma Sintering}, volume={17}, ISSN={2044-5326}, url={http://dx.doi.org/10.1557/jmr.2002.0081}, DOI={10.1557/jmr.2002.0081}, number={3}, journal={Journal of Materials Research}, publisher={Springer Science and Business Media LLC}, author={Takeuchi, Tomonari and Capiglia, Claudio and Balakrishnan, Nalini and Takeda, Yasuo and Kageyama, Hiroyuki}, year={2002}, month=mar, pages={575–581} }

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