Abstract
Preparation of the superconducting oxide, YBa2Cu3O7−x, was carried out according to the metal alkoxide method. To obtain a homogeneous solution of yttrium, barium, and copper alkoxide in an organic solvent, alkoxides of copper and yttrium were modified by the O-R interchange reaction with 2-dimethylaminoethanol and the structures of their modified alkoxides were studied by 1H-NMR, FT-IR, and EXAFS. The YBa2Cu3O7−x precursor, prepared by hydrolysis of the present solution of alkoxides, was calcined at 850°C for 3 h to give YBa2Cu3O7−x powder as a single phase. This powder was sintered between 900°C and 950°C and characterized for bulk density, microstructure, Tc, and Jc.
References
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Dates
Type | When |
---|---|
Created | 17 years, 11 months ago (Sept. 27, 2007, 5:49 a.m.) |
Deposited | 4 years, 6 months ago (Feb. 24, 2021, 4:29 p.m.) |
Indexed | 1 month, 3 weeks ago (July 7, 2025, 9:07 a.m.) |
Issued | 35 years, 4 months ago (April 1, 1990) |
Published | 35 years, 4 months ago (April 1, 1990) |
Published Online | 14 years, 6 months ago (Jan. 31, 2011) |
Published Print | 35 years, 4 months ago (April 1, 1990) |
@article{Katayama_1990, title={Superconducting oxide YBa2Cu3O7−x prepared by the metal alkoxide method}, volume={5}, ISSN={2044-5326}, url={http://dx.doi.org/10.1557/jmr.1990.0683}, DOI={10.1557/jmr.1990.0683}, number={4}, journal={Journal of Materials Research}, publisher={Springer Science and Business Media LLC}, author={Katayama, Shingo and Sekine, Masahiro}, year={1990}, month=apr, pages={683–690} }