DOI: 10.1246/cl.2010.832. Fine Tuning of Pd0 Nanoparticle Formation on Hydroxyapatite and Its Application for Regioselective Quinoline Hydrogenation

Fine Tuning of Pd0 Nanoparticle Formation on Hydroxyapatite and Its Application for Regioselective Quinoline Hydrogenation

10.1246/cl.2010.832

Crossref journal-article

Oxford University Press (OUP)

Chemistry Letters (286)

Abstract

Abstract Fine control of the formation of Pd0 nanoparticles with diameters between 1 and 1.5 nm on hydroxyapatite (HAP) was achieved by adjusting the temperature at which the PdII species on the HAP surface (PdIIHAP) was reduced in the presence of 1 atm of molecular hydrogen. The HAP-supported Pd0 nanoparticles (Pd0HAP) having an average diameter of 1.5 nm exhibited significantly high catalytic activity for the regioselective hydrogenation of quinolines to the corresponding 1,2,3,4-tetrahydroquinolines under mild reaction conditions. Moreover, the Pd0HAP catalyst was reusable without appreciable loss of its high catalytic activity or selectivity.

Bibliography

Hashimoto, N., Takahashi, Y., Hara, T., Shimazu, S., Mitsudome, T., Mizugaki, T., Jitsukawa, K., & Kaneda, K. (2010). Fine Tuning of Pd0 Nanoparticle Formation on Hydroxyapatite and Its Application for Regioselective Quinoline Hydrogenation. Chemistry Letters, 39(8), 832â834.

Authors 8

Norifumi Hashimoto (first)
Yusuke Takahashi (additional)
Takayoshi Hara (additional)
Shogo Shimazu (additional)
Takato Mitsudome (additional)
Tomoo Mizugaki (additional)
Koichiro Jitsukawa (additional)
Kiyotomi Kaneda (additional)

References 35 Referenced 49

Dates

Type	When
Created	15 years, 2 months ago (June 28, 2010, 2:06 a.m.)
Deposited	1 year, 7 months ago (Jan. 18, 2024, 11:30 a.m.)
Indexed	1 year, 3 months ago (May 27, 2024, 11:09 a.m.)
Issued	15 years, 2 months ago (June 26, 2010)
Published	15 years, 2 months ago (June 26, 2010)
Published Online	15 years, 2 months ago (June 26, 2010)
Published Print	15 years, 1 month ago (Aug. 5, 2010)

Funders 0

None

BibTeX

@article{Hashimoto_2010, title={Fine Tuning of Pd0 Nanoparticle Formation on Hydroxyapatite and Its Application for Regioselective Quinoline Hydrogenation}, volume={39}, ISSN={1348-0715}, url={http://dx.doi.org/10.1246/cl.2010.832}, DOI={10.1246/cl.2010.832}, number={8}, journal={Chemistry Letters}, publisher={Oxford University Press (OUP)}, author={Hashimoto, Norifumi and Takahashi, Yusuke and Hara, Takayoshi and Shimazu, Shogo and Mitsudome, Takato and Mizugaki, Tomoo and Jitsukawa, Koichiro and Kaneda, Kiyotomi}, year={2010}, month=jun, pages={832–834} }

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