Abstract
Problems associated with trace hydrogen detection by SIMS are discussed. These include: (1) residual gas contamination, (2) primary ion beam contamination, (3) detection of stray H secondary ions, (4) instrumental background at low mass (for quadrupole instruments), and (5) matrix-related sensitivity artifacts. In depth-profiling a proton implanted silicon sample, H detection limits of <2 × 1018 at/cm3 could be obtained, but only when the partial pressure of H2O was reduced to <1 × 10−10 Torr (1.33 × 10−8 Pa). The importance of using cesium primary ion bombardment is also discussed, as well as the ability to detect both hydrogen and deuterium in the same analysis.
Dates
Type | When |
---|---|
Created | 23 years, 1 month ago (July 27, 2002, 5:33 a.m.) |
Deposited | 2 years, 2 months ago (June 28, 2023, 6:53 p.m.) |
Indexed | 3 days, 20 hours ago (Aug. 27, 2025, 11:47 a.m.) |
Issued | 44 years, 3 months ago (May 1, 1981) |
Published | 44 years, 3 months ago (May 1, 1981) |
Published Print | 44 years, 3 months ago (May 1, 1981) |
@article{Magee_1981, title={Hydrogen depth profiling using SIMS—Problems and their solutions}, volume={19}, ISSN={0022-5355}, url={http://dx.doi.org/10.1116/1.571015}, DOI={10.1116/1.571015}, number={1}, journal={Journal of Vacuum Science and Technology}, publisher={American Vacuum Society}, author={Magee, C. W. and Botnick, E.M.}, year={1981}, month=may, pages={47–52} }