DOI: 10.1111/j.1151-2916.1990.tb06485.x. Lead Zirconate Titanate Fiber/Polymer Composites Prepared by a Replication Process

Lead Zirconate Titanate Fiber/Polymer Composites Prepared by a Replication Process

10.1111/j.1151-2916.1990.tb06485.x

Crossref journal-article

Wiley

Journal of the American Ceramic Society (311)

Abstract

The woven replication process was used to fabricate lead zirconate titanate (PZT)/polymer composites with 1–3, 2–3, and 3–3 connectivities by starting with novoloid‐derived carbon fiber, woven fabric, and nonwoven felt templates, respectively. Activated carbon‐fiber template material was impregnated with PZT by soaking it in a solution containing stoichiometric amounts of dissolved lead, zirconium, titanium, and niobium ions. Heat treatment burned out the carbon, leaving a PZT replica with the same form as the template material. Replicas were sintered in a controlled atmosphere and backfilled with an epoxy polymer to form final composites. This method, which is believed to be adaptable for mass production, is capable of producing composites with extremely fine microstructures. Woven composite samples have fiber tow diameters of 200 to 250 μm and spacings between tows of about 150 to 250 μm. Average d33= 90 pC/N, g33= 211 mV · m/N, and dhgh hydrophone figure of merit of 2100 × 10−15 m2/N values are reported for woven PZT/polymer composites.

Bibliography

Waller, D. J., Safari, A., Card, R. J., & OâToole, M. P. (1990). Lead Zirconate Titanate Fiber/Polymer Composites Prepared by a Replication Process. Journal of the American Ceramic Society, 73(11), 3503â3506. Portico.

Authors 4

David J. Waller (first)
Ahmad Safari (additional)
Roger J. Card (additional)
Michael P. O'Toole (additional)

References 20 Referenced 37

10.1016/0025-5408(80)90090-2
{'key': 'e_1_2_1_3_2', 'first-page': '501', 'article-title': '“Flexible Composite Piezoelectric Sensors,”', 'volume': '1984', 'author': 'Newnham R. E.', 'year': '1984', 'journal-title': 'Ultrason. Symp. Proc.'} / Ultrason. Symp. Proc. / “Flexible Composite Piezoelectric Sensors,” by Newnham R. E. (1984)
{'key': 'e_1_2_1_4_2', 'first-page': '181', 'article-title': '“Hydrophone Figure of Merit,”', 'volume': '4', 'author': 'Bhalla A. S.', 'year': '1988', 'journal-title': 'Sens. Mater.'} / Sens. Mater. / “Hydrophone Figure of Merit,” by Bhalla A. S. (1988)
{'key': 'e_1_2_1_5_2', 'first-page': '92', 'volume-title': 'Electronic Ceramics', 'author': 'Gururaja T. R.', 'year': '1988'} / Electronic Ceramics by Gururaja T. R. (1988)
10.1016/0025-5408(78)90185-X
10.1111/j.1151-2916.1981.tb09549.x
10.1080/00150198208210624
10.1016/0025-5408(81)90267-1
10.1080/00150198108219625
{'key': 'e_1_2_1_11_2', 'first-page': '539', 'article-title': '“Properties of Composite Piezoelectric Materials for Ultrasonic Transducers,”', 'volume': '1984', 'author': 'Smith W. A.', 'year': '1984', 'journal-title': 'Ultrason. Symp. Proc.'} / Ultrason. Symp. Proc. / “Properties of Composite Piezoelectric Materials for Ultrasonic Transducers,” by Smith W. A. (1984)
{'key': 'e_1_2_1_12_2', 'first-page': '645', 'article-title': '“Fired 0–3 Piezoelectric Composite Materials for Biomedical Imaging Applications,”', 'volume': '1987', 'author': 'Madhaven C.', 'year': '1987', 'journal-title': 'Ultrason. Symp. Proc.'} / Ultrason. Symp. Proc. / “Fired 0–3 Piezoelectric Composite Materials for Biomedical Imaging Applications,” by Madhaven C. (1987)
{'key': 'e_1_2_1_13_2', 'first-page': '507', 'article-title': '“Medical Ultrasonic Probe Using PZT/Polymer Composite,”', 'volume': '1984', 'author': 'Takeuchi H.', 'year': '1984', 'journal-title': 'Ultrason. Symp. Proc.'} / Ultrason. Symp. Proc. / “Medical Ultrasonic Probe Using PZT/Polymer Composite,” by Takeuchi H. (1984)
10.1080/00150198608238737
{'key': 'e_1_2_1_15_2', 'first-page': '533', 'article-title': '“Ultrasonic Properties of Piezoelectric PZT Rod–Polymer Composites,”', 'volume': '1984', 'author': 'Gururaja T. R.', 'year': '1984', 'journal-title': 'Ultrason. Symp. Proc.'} / Ultrason. Symp. Proc. / “Ultrasonic Properties of Piezoelectric PZT Rod–Polymer Composites,” by Gururaja T. R. (1984)
10.1109/T-SU.1985.31624
10.1016/0025-5408(78)90161-7
A.Safari “Perforated PZT/Polymer Composites with 3–1 and 3–2 Connectivity for Hydrophone Applications”;Ph.D. Thesis.Solid State Science Pennsylvania State University University Park PA 1983.
10.1111/j.1551-2916.1988.tb00164.x
10.1111/j.1151-2916.1990.tb06569.x
R. J.Card M. P.O'Toole andA.Safari “Method of Making Piezoelectric Composites ”U.S. Pat. No. 4 726 099 1988.

Dates

Type	When
Created	20 years, 5 months ago (March 8, 2005, 12:25 p.m.)
Deposited	1 year, 9 months ago (Nov. 22, 2023, 9:31 p.m.)
Indexed	2 months, 2 weeks ago (June 16, 2025, 8:08 a.m.)
Issued	34 years, 10 months ago (Nov. 1, 1990)
Published	34 years, 10 months ago (Nov. 1, 1990)
Published Online	20 years, 5 months ago (March 8, 2005)
Published Print	34 years, 10 months ago (Nov. 1, 1990)

Funders 0

None

BibTeX

@article{Waller_1990, title={Lead Zirconate Titanate Fiber/Polymer Composites Prepared by a Replication Process}, volume={73}, ISSN={1551-2916}, url={http://dx.doi.org/10.1111/j.1151-2916.1990.tb06485.x}, DOI={10.1111/j.1151-2916.1990.tb06485.x}, number={11}, journal={Journal of the American Ceramic Society}, publisher={Wiley}, author={Waller, David J. and Safari, Ahmad and Card, Roger J. and O’Toole, Michael P.}, year={1990}, month=nov, pages={3503–3506} }

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