DOI: 10.1063/1.4729562. Polymer induced changes of the crystallization scenario in suspensions of hard sphere like microgel particles

Polymer induced changes of the crystallization scenario in suspensions of hard sphere like microgel particles

10.1063/1.4729562

Crossref journal-article

AIP Publishing

The Journal of Chemical Physics (317)

Abstract

We investigated the crystallization scenario of highly cross linked polystyrene particles dispersed in the good solvent 2-ethylnaphtalene and their mixtures with non-adsorbing low molecular weight polysterene polymer using time resolved static light scattering. The samples were prepared slightly below the melting volume fraction of the polymer free system. For the polymer free samples, we obtained polycrystalline solids via crystallization scenario known from hard sphere suspensions with little competition of wall crystal formation. Addition of non-adsorbing low molecular weight polystyrene polymer leads to a considerably slowing down of the bulk crystallization kinetics. We observed a delay of the precursor to crystal conversion for the bulk crystallization while the induction times for the wall nucleation are reduced. The increased polymer concentration thus shifts the balance between the two competing crystallization pathways giving the possibility to tune the relative amount of wall based crystals.

Bibliography

Beyer, R., Iacopini, S., Palberg, T., & SchÃ¶pe, H. J. (2012). Polymer induced changes of the crystallization scenario in suspensions of hard sphere like microgel particles. The Journal of Chemical Physics, 136(23).

Authors 4

Richard Beyer (first)
Sara Iacopini (additional)
Thomas Palberg (additional)
Hans Joachim Schöpe (additional)

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Dates

Type	When
Created	13 years, 2 months ago (June 21, 2012, 8:57 a.m.)
Deposited	2 years, 2 months ago (July 1, 2023, 10:46 p.m.)
Indexed	1 month, 1 week ago (July 30, 2025, 6:59 a.m.)
Issued	13 years, 2 months ago (June 20, 2012)
Published	13 years, 2 months ago (June 20, 2012)
Published Online	13 years, 2 months ago (June 20, 2012)
Published Print	13 years, 2 months ago (June 21, 2012)

Funders 2

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BibTeX

@article{Beyer_2012, title={Polymer induced changes of the crystallization scenario in suspensions of hard sphere like microgel particles}, volume={136}, ISSN={1089-7690}, url={http://dx.doi.org/10.1063/1.4729562}, DOI={10.1063/1.4729562}, number={23}, journal={The Journal of Chemical Physics}, publisher={AIP Publishing}, author={Beyer, Richard and Iacopini, Sara and Palberg, Thomas and Schöpe, Hans Joachim}, year={2012}, month=jun }

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