Crossref journal-article
AIP Publishing
The Journal of Chemical Physics (317)
Abstract

The effects of homonuclear dipole couplings may be reintroduced into magic angle spinning nuclear magnetic resonance (NMR) spectra by judiciously spaced π pulse trains. This recoupling phenomenon occurs over a wide range of chemical shift differences and sample rotation speeds. We present results of magnetization exchange experiments exploiting the broad band recoupling effect, and propose a theoretical description in which pulse-assisted dipolar recoupling may be understood as a form of compensated rotational resonance.

Bibliography

Sodickson, D. K., Levitt, M. H., Vega, S., & Griffin, R. G. (1993). Broad band dipolar recoupling in the nuclear magnetic resonance of rotating solids. The Journal of Chemical Physics, 98(9), 6742–6748.

Authors 4
  1. D. K. Sodickson (first)
  2. M. H. Levitt (additional)
  3. S. Vega (additional)
  4. R. G. Griffin (additional)
References 27 Referenced 86
  1. {'key': '2024021101503216800_r1'}
  2. 10.1103/PhysRevB.32.5608 / Phys. Rev. B (1985)
  3. {'key': '2024021101503216800_r2a', 'first-page': '6038', 'volume': '25', 'year': '1985', 'journal-title': 'Phys. Rev. B'} / Phys. Rev. B (1985)
  4. 10.1063/1.458314 / J. Chem. Phys. (1990)
  5. 10.1016/0009-2614(88)85051-6 / Chem. Phys. Lett. (1988)
  6. 10.1016/0009-2614(90)87235-J / Chem. Phys. Lett. (1990)
  7. {'key': '2024021101503216800_r6'}
  8. {'key': '2024021101503216800_r7'}
  9. 10.1016/0009-2614(92)85790-H / Chem. Phys. Lett. (1992)
  10. 10.1063/1.462267 / J. Chem. Phys. (1992)
  11. {'key': '2024021101503216800_r10', 'first-page': '88', 'volume': '55', 'year': '1983', 'journal-title': 'J. Magn. Reson.'} / J. Magn. Reson. (1983)
  12. {'key': '2024021101503216800_r11'}
  13. {'key': '2024021101503216800_r12', 'first-page': '479', 'volume': '89', 'year': '1990', 'journal-title': 'J. Magn. Reson.'} / J. Magn. Reson. (1990)
  14. {'key': '2024021101503216800_r13'}
  15. 10.1063/1.435679 / J. Chem. Phys. (1978)
  16. 10.1063/1.435038 / J. Chem. Phys. (1977)
  17. {'key': '2024021101503216800_r16'}
  18. 10.1063/1.460398 / J. Chem. Phys. (1991)
  19. {'key': '2024021101503216800_r18'}
  20. {'key': '2024021101503216800_r19', 'first-page': '521', 'volume': '53', 'year': '1983', 'journal-title': 'J. Magn. Reson.'} / J. Magn. Reson. (1983)
  21. {'key': '2024021101503216800_r20', 'first-page': '196', 'volume': '81', 'year': '1989', 'journal-title': 'J. Magn. Reson.'} / J. Magn. Reson. (1989)
  22. {'key': '2024021101503216800_r21'}
  23. {'key': '2024021101503216800_r22', 'first-page': '4502', 'volume': '11', 'year': '1989', 'journal-title': 'J. Am. Chem. Soc.'} / J. Am. Chem. Soc. (1989)
  24. 10.1021/bi00476a018 / Biochem. (1990)
  25. 10.1126/science.1990439 / Science (1991)
  26. {'key': '2024021101503216800_r25', 'first-page': '10', 'volume': '30', 'year': '1991', 'journal-title': 'Biochem.'} / Biochem. (1991)
  27. 10.1021/bi00149a026 / Biochem. (1992)
Dates
Type When
Created 23 years, 1 month ago (July 26, 2002, 8:22 a.m.)
Deposited 1 year, 6 months ago (Feb. 10, 2024, 8:50 p.m.)
Indexed 1 month, 1 week ago (July 26, 2025, 4:40 a.m.)
Issued 32 years, 4 months ago (May 1, 1993)
Published 32 years, 4 months ago (May 1, 1993)
Published Print 32 years, 4 months ago (May 1, 1993)
Funders 0

None

@article{Sodickson_1993, title={Broad band dipolar recoupling in the nuclear magnetic resonance of rotating solids}, volume={98}, ISSN={1089-7690}, url={http://dx.doi.org/10.1063/1.464766}, DOI={10.1063/1.464766}, number={9}, journal={The Journal of Chemical Physics}, publisher={AIP Publishing}, author={Sodickson, D. K. and Levitt, M. H. and Vega, S. and Griffin, R. G.}, year={1993}, month=may, pages={6742–6748} }