DOI: 10.1063/1.354256. Raman spectroscopy, x-ray diffraction, and phase relationship determinations with a versatile heating cell for measurements up to 3600 K (or 2700 K in air)

Raman spectroscopy, x-ray diffraction, and phase relationship determinations with a versatile heating cell for measurements up to 3600 K (or 2700 K in air)

10.1063/1.354256

Crossref journal-article

AIP Publishing

Journal of Applied Physics (317)

Abstract

A simple, rapid, and inexpensive heating-wire technique is used for physical observations at high temperatures. The upper limit is 2000 K in air with platinum-iridium or platinum-rhodium wires and 2700 K with iridium; temperatures up to 3600 K can be achieved under an inert atmosphere with tungsten wires. Raman spectroscopy measurements made up to 1900 K by this technique suggest that the high-temperature harmonic vibrational behavior of corundum (α-Al2O3) results from the cancellation of anharmonic effects. Powder x-ray diffraction experiments with synchrotron radiation show that perovskite (CaTiO3) changes from orthorhombic symmetry to cubic between 1330 and 1530 K, with an intermediate tetragonal phase likely, consistent with λ-type transitions recorded by recent calorimetric measurements. Finally, observations of CaAl2Si2O8 polymorphism has shown the existence of a new metastable phase.

Bibliography

Richet, P., Gillet, P., Pierre, A., Bouhifd, M. A., Daniel, I., & Fiquet, G. (1993). Raman spectroscopy, x-ray diffraction, and phase relationship determinations with a versatile heating cell for measurements up to 3600 K (or 2700 K in air). Journal of Applied Physics, 74(9), 5451â5456.

Authors 6

Pascal Richet (first)
Philippe Gillet (additional)
Alain Pierre (additional)
M. Ali Bouhifd (additional)
Isabelle Daniel (additional)
Guillaume Fiquet (additional)

References 17 Referenced 59

10.1016/0009-2541(92)90062-A / Chem. Geol. (1992)
10.1029/90JB02172 / J. Geophys. Res. (1991)
10.6028/jres.087.012 / J. Res. Natl. Bur. Stand. (1982)
10.1029/91RG02810 / Rev. Geophys. (1992)
10.1103/PhysRevB.7.2779 / Phys. Rev. B (1973)
10.1029/91JB00680 / J. Geophys. Res. (1991)
10.1063/1.328785 / J. Appl. Phys. (1981)
{'key': '2024020211362826800_r8', 'first-page': '98', 'volume': '10', 'year': '1992', 'journal-title': 'Adv. Phys. Geochem.'} / Adv. Phys. Geochem. (1992)
10.1080/00150197608237799 / Ferroelectrics (1976)
10.1080/00150197808239430 / Ferroelectrics (1978)
10.1021/ja01210a030 / J. Am. Chem. Soc. (1946)
{'key': '2024020211362826800_r12'}
{'key': '2024020211362826800_r13', 'first-page': '107', 'volume': '250A', 'year': '1952', 'journal-title': 'Am. J. Sci.'} / Am. J. Sci. (1952)
{'key': '2024020211362826800_r14', 'first-page': '473', 'volume': '17', 'year': '1991', 'journal-title': 'Phys. Chem. Miner.'} / Phys. Chem. Miner. (1991)
10.1016/0012-821X(84)90179-1 / Earth Planet Sci. Lett. (1984)
{'key': '2024020211362826800_r16'}
{'key': '2024020211362826800_r17', 'volume': '1452', 'year': '1979', 'journal-title': 'US Geolog. Surv. Bull.'} / US Geolog. Surv. Bull. (1979)

Dates

Type	When
Created	23 years ago (July 26, 2002, 8:39 a.m.)
Deposited	1 year, 6 months ago (Feb. 2, 2024, 7:13 a.m.)
Indexed	1 year, 6 months ago (Feb. 10, 2024, 11:07 a.m.)
Issued	31 years, 9 months ago (Nov. 1, 1993)
Published	31 years, 9 months ago (Nov. 1, 1993)
Published Print	31 years, 9 months ago (Nov. 1, 1993)

Funders 0

None

BibTeX

@article{Richet_1993, title={Raman spectroscopy, x-ray diffraction, and phase relationship determinations with a versatile heating cell for measurements up to 3600 K (or 2700 K in air)}, volume={74}, ISSN={1089-7550}, url={http://dx.doi.org/10.1063/1.354256}, DOI={10.1063/1.354256}, number={9}, journal={Journal of Applied Physics}, publisher={AIP Publishing}, author={Richet, Pascal and Gillet, Philippe and Pierre, Alain and Bouhifd, M. Ali and Daniel, Isabelle and Fiquet, Guillaume}, year={1993}, month=nov, pages={5451–5456} }

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