DOI: 10.1063/1.2965470. Local thermomechanical characterization of phase transitions using band excitation atomic force acoustic microscopy with heated probe

Local thermomechanical characterization of phase transitions using band excitation atomic force acoustic microscopy with heated probe

10.1063/1.2965470

Crossref journal-article

AIP Publishing

Applied Physics Letters (317)

Abstract

An approach for thermomechanical characterization of phase transitions in polymeric materials (polyethyleneterephthalate) by band excitation acoustic force microscopy is developed. This methodology allows the independent measurement of resonance frequency, Q factor, and oscillation amplitude of a tip-surface contact as a function of tip temperature, from which the thermal evolution of tip-surface spring constant and mechanical dissipation can be extracted. We demonstrate a heating protocol which keeps the contact area and contact force constant, thus allowing for reproducible measurements and quantitative extraction of material properties including temperature dependence of indentation-based elastic and loss moduli.

Bibliography

Jesse, S., Nikiforov, M. P., Germinario, L. T., & Kalinin, S. V. (2008). Local thermomechanical characterization of phase transitions using band excitation atomic force acoustic microscopy with heated probe. Applied Physics Letters, 93(7).

Authors 4

S. Jesse (first)
M. P. Nikiforov (additional)
L. T. Germinario (additional)
S. V. Kalinin (additional)

References 17 Referenced 42

10.1126/science.1151205 / Science (2008)
10.1103/PhysRevLett.85.2340 / Phys. Rev. Lett. (2000)
10.1016/S0040-6031(02)00113-2 / Thermochim. Acta (2002)
10.1016/S0040-6031(00)00552-9 / Thermochim. Acta (2000)
10.1002/jps.10103 / J. Pharm. Sci. (2002)
10.1063/1.2435589 / Rev. Sci. Instrum. (2007)
10.1063/1.111869 / Appl. Phys. Lett. (1994)
10.1063/1.1147409 / Rev. Sci. Instrum. (1996)
10.1088/0957-4484/18/43/435503 / Nanotechnology (2007)
10.1557/jmr.2004.19.1.3 / J. Mater. Res. (2004)
{'volume-title': 'Time-Frequency Analysis', 'year': '1995', 'key': '2023070220391478400_c9'} / Time-Frequency Analysis (1995)
10.1109/JMEMS.2006.886020 / J. Microelectromech. Syst. (2006)
10.1016/j.sna.2007.06.008 / Sens. Actuators, A (2007)
{'volume-title': 'Exploring Scanning Probe Microscopy with Mathematica', 'year': '1997', 'key': '2023070220391478400_c12'} / Exploring Scanning Probe Microscopy with Mathematica (1997)
10.1063/1.2221496 / Appl. Phys. Lett. (2006)
10.1063/1.2801524 / Appl. Phys. Lett. (2008)
10.1063/1.2818805 / Rev. Sci. Instrum. (2007)

Dates

Type	When
Created	17 years ago (Aug. 21, 2008, 12:23 a.m.)
Deposited	2 years, 1 month ago (July 2, 2023, 4:39 p.m.)
Indexed	3 weeks, 1 day ago (July 30, 2025, 6:51 a.m.)
Issued	17 years ago (Aug. 18, 2008)
Published	17 years ago (Aug. 18, 2008)
Published Online	17 years ago (Aug. 19, 2008)
Published Print	17 years ago (Aug. 18, 2008)

Funders 0

None

BibTeX

@article{Jesse_2008, title={Local thermomechanical characterization of phase transitions using band excitation atomic force acoustic microscopy with heated probe}, volume={93}, ISSN={1077-3118}, url={http://dx.doi.org/10.1063/1.2965470}, DOI={10.1063/1.2965470}, number={7}, journal={Applied Physics Letters}, publisher={AIP Publishing}, author={Jesse, S. and Nikiforov, M. P. and Germinario, L. T. and Kalinin, S. V.}, year={2008}, month=aug }

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