DOI: 10.1063/1.1684141. A Drop Calorimeter with an Electron Beam Heated Furnace

A Drop Calorimeter with an Electron Beam Heated Furnace

10.1063/1.1684141

Crossref journal-article

AIP Publishing

Review of Scientific Instruments (317)

Abstract

The design and operation of a calorimetric system for the measurement of high temperature enthalpy by the method of mixtures, or ``drop method,'' is described. Features of the system are (1) an electron beam heated furnace, with sample temperatures determined by optical pyrometry, (2) a copper block calorimeter with calorimeter temperatures obtained by quartz crystal thermometry, and (3) provision for pneumatic acceleration of the sample from the furnace into the calorimeter to minimize heat losses during the transfer. The system has been used to measure the enthalpy of tungsten in the temperature range 1300–1900 K. Values agree with literature data to ±0.5%.

Bibliography

Fredrickson, D. R., Kleb, R., Nuttall, R. L., & Hubbard, W. N. (1969). A Drop Calorimeter with an Electron Beam Heated Furnace. Review of Scientific Instruments, 40(8), 1022â1025.

Authors 4

D. R. Fredrickson (first)
R. Kleb (additional)
R. L. Nuttall (additional)
W. N. Hubbard (additional)

References 15 Referenced 7

10.1021/ja01856a072 / J. Amer. Chem. Soc. (1941)
10.6028/jres.057.008 / J. Res. Nat. Bur. Stand. (1956)
10.1063/1.1746630 / Rev. Sci. Instrum. (1962)
{'key': '2024020611224645800_r4', 'first-page': '3', 'volume': '4', 'year': '1961', 'journal-title': 'Inzh.-Fiz. Zh.'} / Inzh.-Fiz. Zh. (1961)
{'key': '2024020611224645800_r4a'}
10.1021/j100823a033 / J. Phys. Chem. (1961)
10.1021/j150569a021 / J. Phys. Chem. (1958)
{'key': '2024020611224645800_r7'}
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Dates

Type	When
Created	21 years, 6 months ago (Feb. 10, 2004, 4:49 p.m.)
Deposited	1 year, 6 months ago (Feb. 6, 2024, 6:53 a.m.)
Indexed	1 year, 2 months ago (June 12, 2024, 9:59 a.m.)
Issued	56 years, 1 month ago (Aug. 1, 1969)
Published	56 years, 1 month ago (Aug. 1, 1969)
Published Print	56 years, 1 month ago (Aug. 1, 1969)

Funders 0

None

BibTeX

@article{Fredrickson_1969, title={A Drop Calorimeter with an Electron Beam Heated Furnace}, volume={40}, ISSN={1089-7623}, url={http://dx.doi.org/10.1063/1.1684141}, DOI={10.1063/1.1684141}, number={8}, journal={Review of Scientific Instruments}, publisher={AIP Publishing}, author={Fredrickson, D. R. and Kleb, R. and Nuttall, R. L. and Hubbard, W. N.}, year={1969}, month=aug, pages={1022–1025} }

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