Abstract
The design and construction details of a kW power level pulsed EPR spectrometer with an 8–18 GHz frequency range are presented. The spectrometer is designed for high sensitivity over this wide frequency range. A synthesized sweeper is used as the microwave source. Details of the pulse electronics, pulse timings, cryogenics, and the Macintosh computer interface are described. Representative three pulse electron spin echo envelope modulation patterns of a Cu (II) tetraimidazole complex at X- and P-band frequencies are presented.
References
26
Referenced
52
{'key': '2024020714245409500_r1'}
{'key': '2024020714245409500_r2'}
{'key': '2024020714245409500_r3'}
10.1002/anie.199102651
/ Chem. Int. Ed. Engl. (1991)10.1002/ijch.198800035
/ Isr. J. Chem. (1988)10.1063/1.453782
/ J. Chem. Phys. (1988)10.1063/1.1139373
/ Rev. Sci. Instrum. (1987)10.1021/bi00662a033
/ Biochemistry (1976)10.1063/1.1686567
/ Rev. Sci. Instrum. (1974)10.1016/B978-0-12-005217-2.50015-4
/ Adv. Biol. Med. Phys. (1980)10.1021/j100489a013
/ J. Phys. Chem. (1979)10.1021/ja00247a037
/ J. Am. Chem. Soc. (1987)10.1063/1.1137749
/ Rev. Sci. Instrum. (1984)10.1021/ja00192a006
/ J. Am. Chem. Soc. (1989){'key': '2024020714245409500_r15', 'first-page': '74', 'volume': '66', 'year': '1986', 'journal-title': 'J. Magn. Reson.'}
/ J. Magn. Reson. (1986){'key': '2024020714245409500_r16', 'first-page': '119', 'volume': '8', 'year': '1990', 'journal-title': 'Spectros. Int. J.'}
/ Spectros. Int. J. (1990)10.1063/1.1141584
/ Rev. Sci. Instrum. (1990)10.1063/1.453532
/ J. Chem. Phys. (1987)10.1063/1.455293
/ J. Chem. Phys. (1988){'key': '2024020714245409500_r20'}
{'key': '2024020714245409500_r21'}
{'key': '2024020714245409500_r22'}
{'key': '2024020714245409500_r23', 'first-page': '535', 'volume': '74', 'year': '1987', 'journal-title': 'J. Magn. Reson.'}
/ J. Magn. Reson. (1987)10.1063/1.1717463
/ Rev. Sci. Instrum. (1961){'key': '2024020714245409500_r25', 'first-page': '515', 'volume': '47', 'year': '1982', 'journal-title': 'J. Magn. Reson.'}
/ J. Magn. Reson. (1982)10.1063/1.436479
/ J. Chem. Phys. (1978)
Dates
Type | When |
---|---|
Created | 23 years, 1 month ago (July 26, 2002, 9:57 a.m.) |
Deposited | 1 year, 6 months ago (Feb. 7, 2024, 4:03 p.m.) |
Indexed | 4 weeks ago (Aug. 6, 2025, 8:26 a.m.) |
Issued | 33 years, 5 months ago (April 1, 1992) |
Published | 33 years, 5 months ago (April 1, 1992) |
Published Print | 33 years, 5 months ago (April 1, 1992) |
@article{Sturgeon_1992, title={Sensitive pulsed EPR spectrometer with an 8–18 GHz frequency range}, volume={63}, ISSN={1089-7623}, url={http://dx.doi.org/10.1063/1.1143136}, DOI={10.1063/1.1143136}, number={4}, journal={Review of Scientific Instruments}, publisher={AIP Publishing}, author={Sturgeon, Bradley E. and Britt, R. David}, year={1992}, month=apr, pages={2187–2192} }