DOI: 10.1063/1.104865. Preparation of high-purity Tl-based ‘‘1223’’ superconductor phase by modified Pechini process in water solution

Preparation of high-purity Tl-based ‘‘1223’’ superconductor phase by modified Pechini process in water solution

10.1063/1.104865

Crossref journal-article

AIP Publishing

Applied Physics Letters (317)

Abstract

Because of the mixed metal valance state of thallium in a Tl-based superconductor, a nearly single ‘‘1223’’ phase can be readily prepared by a modified Pechini method (US Patent 3 330 697). Tl2O3 and other metal nitrates are dissolved in an aqueous solution plus a certain amount of oxalic acid for chelating the metal cations. The desired phase shows zero resistance at 114 K and the phase purity is identified by x-ray diffraction. Characteristics of superconductivity also are evidenced by the Meissner effect. The preparation technique is considered valuable to purify multiphase superconductors for mass production.

Bibliography

Chiang, C., Shei, C. Y., Wu, S. F., & Huang, Y. T. (1991). Preparation of high-purity Tl-based ââ1223ââ superconductor phase by modified Pechini process in water solution. Applied Physics Letters, 58(21), 2435â2437.

Authors 4

Cyril Chiang (first)
C. Y. Shei (additional)
S. F. Wu (additional)
Y. T. Huang (additional)

References 19 Referenced 12

10.1143/JJAP.27.2062 / Jpn. J. Appl. Phys. (1988)
10.1126/science.242.4876.249 / Science (1988)
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{'key': '2024020302251551100_r4', 'first-page': 'L', 'volume': '28', 'year': '1989', 'journal-title': 'Jpn. J. Appl. Phys.'} / Jpn. J. Appl. Phys. (1989)
10.1063/1.103174 / Appl. Phys. Lett. (1990)
10.1063/1.103315 / Appl. Phys. Lett. (1990)
10.1063/1.104171 / Appl. Phys. Lett. (1990)
10.1016/0921-4534(90)90616-M / Physica C (1990)
{'key': '2024020302251551100_r9', 'first-page': 'L', 'volume': '29', 'year': '1990', 'journal-title': 'Jpn. J. Appl. Phys.'} / Jpn. J. Appl. Phys. (1990)
{'key': '2024020302251551100_r10'}
10.1063/1.103367 / Appl. Phys. Lett. (1990)
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{'key': '2024020302251551100_r15'}
{'key': '2024020302251551100_r16', 'first-page': 'L', 'volume': '27', 'year': '1988', 'journal-title': 'Jpn. J. Appl. Phys.'} / Jpn. J. Appl. Phys. (1988)
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{'key': '2024020302251551100_r18', 'first-page': 'L', 'volume': '28', 'year': '1989', 'journal-title': 'Jpn. J. Appl. Phys.'} / Jpn. J. Appl. Phys. (1989)
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Dates

Type	When
Created	23 years, 1 month ago (July 26, 2002, 9:31 a.m.)
Deposited	1 year, 6 months ago (Feb. 2, 2024, 9:25 p.m.)
Indexed	1 year, 6 months ago (Feb. 2, 2024, 9:43 p.m.)
Issued	34 years, 3 months ago (May 27, 1991)
Published	34 years, 3 months ago (May 27, 1991)
Published Print	34 years, 3 months ago (May 27, 1991)

Funders 0

None

BibTeX

@article{Chiang_1991, title={Preparation of high-purity Tl-based ‘“1223”’ superconductor phase by modified Pechini process in water solution}, volume={58}, ISSN={1077-3118}, url={http://dx.doi.org/10.1063/1.104865}, DOI={10.1063/1.104865}, number={21}, journal={Applied Physics Letters}, publisher={AIP Publishing}, author={Chiang, Cyril and Shei, C. Y. and Wu, S. F. and Huang, Y. T.}, year={1991}, month=may, pages={2435–2437} }

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