DOI: 10.1039/c4fd00229f. Mapping water uptake in organic coatings using AFM-IR

Mapping water uptake in organic coatings using AFM-IR

10.1039/c4fd00229f

Crossref journal-article

Royal Society of Chemistry (RSC)

Faraday Discussions (292)

Abstract

The long-term failure of seemingly intact corrosion resistant organic coatings is thought to occur via the development of ionic transport channels, which spontaneously evolve from hydrophilic regions on immersion, i.e., as a result of localized water uptake. To this end, we investigate water uptake characteristics for industrial epoxy–phenolic can coatings after immersion in deionized water and drying. Moisture sorption and the changing nature of polymer–water interactions are assessed using FTIR for dry and pre-soaked films. More water is found to be absorbed by the pre-soaked coatings on exposure to a humid environment, with a greater degree of hydrogen-bonding between the polymer and water. Furthermore, morphological changes are then correlated to localized water uptake using the AFM-IR technique. Nanoscale softened regions develop on soaking, and these are found to absorb a greater proportion of water from a humid environment.

Bibliography

Morsch, S., Lyon, S., Greensmith, P., Smith, S. D., & Gibbon, S. R. (2015). Mapping water uptake in organic coatings using AFM-IR. Faraday Discussions, 180, 527â542.

Authors 5

S. Morsch (first)
S. Lyon (additional)
P. Greensmith (additional)
S. D. Smith (additional)
S. R. Gibbon (additional)

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Dates

Type	When
Created	10 years, 4 months ago (April 23, 2015, 8:30 a.m.)
Deposited	1 year, 4 months ago (April 17, 2024, 1:49 p.m.)
Indexed	1 month ago (July 27, 2025, 3:24 a.m.)
Issued	10 years, 8 months ago (Jan. 1, 2015)
Published	10 years, 8 months ago (Jan. 1, 2015)
Published Online	10 years, 8 months ago (Jan. 1, 2015)

Funders 0

None

BibTeX

@article{Morsch_2015, title={Mapping water uptake in organic coatings using AFM-IR}, volume={180}, ISSN={1364-5498}, url={http://dx.doi.org/10.1039/c4fd00229f}, DOI={10.1039/c4fd00229f}, journal={Faraday Discussions}, publisher={Royal Society of Chemistry (RSC)}, author={Morsch, S. and Lyon, S. and Greensmith, P. and Smith, S. D. and Gibbon, S. R.}, year={2015}, pages={527–542} }

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  "abstract": "<p>The long-term failure of seemingly intact corrosion resistant organic coatings is thought to occur <italic>via</italic> the development of ionic transport channels, which spontaneously evolve from hydrophilic regions on immersion, <italic>i.e.</italic>, as a result of localized water uptake. To this end, we investigate water uptake characteristics for industrial epoxy\u2013phenolic can coatings after immersion in deionized water and drying. Moisture sorption and the changing nature of polymer\u2013water interactions are assessed using FTIR for dry and pre-soaked films. More water is found to be absorbed by the pre-soaked coatings on exposure to a humid environment, with a greater degree of hydrogen-bonding between the polymer and water. Furthermore, morphological changes are then correlated to localized water uptake using the AFM-IR technique. Nanoscale softened regions develop on soaking, and these are found to absorb a greater proportion of water from a humid environment.</p>",
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