DOI: 10.1021/om980102m. Synthesis and Reactions offac-Re(bpy)(CO)3(CH2OR) (R = H, Acetyl; bpy = 2,2‘-Bipyridyl)

Synthesis and Reactions offac-Re(bpy)(CO)3(CH2OR) (R = H, Acetyl; bpy = 2,2‘-Bipyridyl)

10.1021/om980102m

Crossref journal-article

American Chemical Society (ACS)

Organometallics (316)

Bibliography

Gibson, D. H., Sleadd, B. A., Yin, X., & Vij, A. (1998). Synthesis and Reactions offac-Re(bpy)(CO)3(CH2OR) (R = H, Acetyl; bpy = 2,2â-Bipyridyl). Organometallics, 17(13), 2689â2691.

Authors 4

Dorothy H. Gibson (first)
Bradley A. Sleadd (additional)
Xiaolong Yin (additional)
Ashwani Vij (additional)

References 41 Referenced 23

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{'volume-title': 'Catalytic Activation of Carbon Dioxide', 'year': '1988', 'author': 'Sullivan B. P.', 'key': 'om980102mb00001/om980102mb00001_7'} / Catalytic Activation of Carbon Dioxide by Sullivan B. P. (1988)
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10.1021/ja962168j / J. Am. Chem. Soc. by Gibson D. H. (1996)
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10.1021/ic00046a021 / Inorg. Chem. by Shaver R. J. (1992)
To a solution of Re(bpy)(CO)4OTf 5(0.20 g, 0.35 mmol) in 25 mL of MeOH at 0 °C was added NaBH4(0.058 g, 1.5 mmol) in several portions. The reaction flask was wrapped in Al foil and stirred for 1 h at 0 °C. The solvent was evaporated, and the resultant red solid was collected and washed with water (100 mL). A red solid was obtained (1; 0.11 g, 69%) and dried under vacuum; mp 158−160 °C dec. Anal. Calcd for C14H11N2O4Re: C, 36.76; H, 2.42. Found: C, 36.86; H, 2.47. IR (DRIFTS, KCl): νCO1987 (s), 1865 (vs) cm-1.1H NMR (CD3OD): δ 9.06 (2H, d,J= 5.7 Hz), 8.52 (2H, d,J= 8.4 Hz), 8.12 (2H, t,J= 8.1 Hz), 7.55 (2H, t,J= 7.8 Hz), 3.37 (2H, s).13C NMR (CD3OD): δ 203.98, 194.44, 156.59, 153.74, 139.24, 127.80, 124.68, 70.05.
{'key': 'om980102mb00007/om980102mb00007_1', 'first-page': '1', 'volume': '1997', 'author': 'Compound 0.', 'year': '2017', 'journal-title': 'CO'} / CO by Compound 0. (2017)
{'volume-title': 'mp >210 °C. Anal. Calcd for C14H11N2O4Re:\u2009 C, 36.67', 'year': '2003', 'author': 'The', 'key': 'om980102mb00010/om980102mb00010_1'} / mp >210 °C. Anal. Calcd for C14H11N2O4Re: C, 36.67 by The (2003)
{'volume-title': 'space group P1̄', 'year': '2033', 'author': 'Crystal O', 'key': 'om980102mb00011/om980102mb00011_1'} / space group P1̄ by Crystal O (2033)
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10.1002/hlca.19940770813 / Helv. Chim. Acta by Nietlispach D. (1994)
10.1021/om970079p / Organometallics by Ayllón J. A. (1997)
{'volume-title': 'We obtained better results as follows:\u2009 0.40 g (0.79 mmol) of Re(bpy)(CO)3Br was added to a Schlenk flask under N2', 'author': 'Compound', 'key': 'om980102mb00022/om980102mb00022_1'} / We obtained better results as follows: 0.40 g (0.79 mmol) of Re(bpy)(CO)3Br was added to a Schlenk flask under N2 by Compound
10.1021/jo00186a020 / J. Org. Chem. by Slocum G. H. (1984)
{'volume-title': '6 and another compound believed to be an isomer (the 1H NMR showed an acetoxy methyl resonance at δ 1.91 and resonances for bipyridyl protons which are distinct from 6', 'author': 'Photolysis', 'key': 'om980102mb00024/om980102mb00024_1'} / 6 and another compound believed to be an isomer (the 1H NMR showed an acetoxy methyl resonance at δ 1.91 and resonances for bipyridyl protons which are distinct from 6 by Photolysis
{'key': 'om980102mb00024/om980102mb00024_2', 'first-page': '1', 'volume': '1904', 'author': 'Alternate 0.', 'year': '2018', 'journal-title': 'CO'} / CO by Alternate 0. (2018)
10.1021/ja00087a072 / J. Am. Chem. Soc. by Gogoll A. (1994)
10.1021/om00061a031 / Organometallics by Thorn D. L. (1982)
10.1021/om00072a006 / Organometallics by Thorn D. L. (1982)
10.1021/om50004a039 / Organometallics by Lin Y. C. (1983)

Dates

Type	When
Created	23 years, 1 month ago (July 26, 2002, 1:30 a.m.)
Deposited	8 months, 2 weeks ago (Dec. 7, 2024, 12:05 a.m.)
Indexed	8 months, 2 weeks ago (Dec. 7, 2024, 12:40 a.m.)
Issued	27 years, 3 months ago (May 23, 1998)
Published	27 years, 3 months ago (May 23, 1998)
Published Online	27 years, 3 months ago (May 23, 1998)
Published Print	27 years, 2 months ago (June 1, 1998)

Funders 0

None

BibTeX

@article{Gibson_1998, title={Synthesis and Reactions offac-Re(bpy)(CO)3(CH2OR) (R = H, Acetyl; bpy = 2,2‘-Bipyridyl)}, volume={17}, ISSN={1520-6041}, url={http://dx.doi.org/10.1021/om980102m}, DOI={10.1021/om980102m}, number={13}, journal={Organometallics}, publisher={American Chemical Society (ACS)}, author={Gibson, Dorothy H. and Sleadd, Bradley A. and Yin, Xiaolong and Vij, Ashwani}, year={1998}, month=may, pages={2689–2691} }

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