DOI: 10.1021/ma9703214. Synthesis and Chemistry of Novel Dendritic Macromolecules Possessing Internal Electroactive Anthraquinonoid Moieties

Synthesis and Chemistry of Novel Dendritic Macromolecules Possessing Internal Electroactive Anthraquinonoid Moieties

10.1021/ma9703214

Crossref journal-article

American Chemical Society (ACS)

Macromolecules (316)

Bibliography

Newkome, G. R., Narayanan, V. V., Echegoyen, L., PÃ©rez-Cordero, E., & Luftmann, H. (1997). Synthesis and Chemistry of Novel Dendritic Macromolecules Possessing Internal Electroactive Anthraquinonoid Moieties. Macromolecules, 30(17), 5187â5191.

Authors 5

George R. Newkome (first)
Venkatraj V. Narayanan (additional)
Luis Echegoyen (additional)
Eduardo Pérez-Cordero (additional)
Heinrich Luftmann (additional)

References 35 Referenced 17

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Juris, A.; Venturi, M.; Pontoni, L.; Resino, I. R.; Balzani, V.; Serroni, S.; Campagna, S.; Denti, G.Can. J. Chem.1995,73, 1875; Serroni, S.; Campagna, S.; Denti, G.; Juris, A.; Venturi, M.; Balzani, V. InAdvances inDendritic Macromolecules;Newkome, G. R., Ed.; JAI Press, Inc. Greenwich, CT, 1996; Vol. 3, p 61. (10.1139/v95-232)
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{'key': 'ma9703214b00021/ma9703214b00021_1', 'volume-title': '1 m path length, 200−600 FWHM resolution, and accuracy of mass determination ±0.1%)'} / 1 m path length, 200−600 FWHM resolution, and accuracy of mass determination ±0.1%)
6: 80%, mp 140−142 °C; IR (KBr) 3400 (OH, broad), 1700 (CO) cm-1;13C NMR (DMSO-d6) δ 21.2 (CH2CH2CH2), 29.2, 30.7 (CH2CH2CO2), 35.1, 37.2 (CH2CH2CH2), 45.5 (4°Ccore), 56.4 (NHC4°), 68.0, 69.9 (CH2OCH2), 116.0, 127.7, 132.1, 134.5, 137.1, 137.3 (CAr), 170.3, 171.5, 171.7 (CONH), 174.7 (CO2H), 185.5 (COquin); MALDI-TOF-MSm/z2704 (M + Na). Anal. Calcd for C133H144N12O48: C, 59.64; H, 5.42; N, 6.27. Found: C, 59.42; H, 5.28; N, 6.09.
Bodanszky, M.; Bodanszky, A.The Practice of Peptide Synthesis.Reactivity and Structure Concepts in Organic Chemistry; Springer Verlag: New York, 1984; Vol. 21, p 145. (10.1007/978-3-642-96835-8)
{'key': 'ma9703214b00026/ma9703214b00026_1', 'volume-title': 'bright orange solid, mp 65−69 °C'} / bright orange solid, mp 65−69 °C
Cyclic voltammograms at 20 °C were recorded on a BAS-100-W electrochemical apparatus from Bioanalytical systems, Inc. A conventional three-electrode configuration was used with a 3 mm diameter glassy-carbon disk as the working electrode, a platinum working electrode, and a silver wire pseudo-reference electrode. Electrochemical grade (TBA)PF6was recrystallized (EtOH, 2×) and pulverized. HPLC grade MeCN was dried (P4O10) and vapor transferred directly into the electrochemical cell after three freeze−pump−thaw degassing cycles at 10-5−10-6mm Hg. In general, a 0.5 mL sample solution containing 1 mM metal complex and 100 mM (TBA)PF6was prepared by drying the solid reagents directly in the electrochemical cell at 10-5−10-6mm Hg and then transferring the solvent directly into it through the vacuum line. Micromolar solutions of1,3, and5−8were made in THF and UV spectra obtained on a HP 8452 diode-array spectrophotometer.
10.1002/anie.199520231 / Angew. Chem., Int. Ed. Engl. by Newkome G. R. (1995)
{'key': 'ma9703214b00029/ma9703214b00029_1', 'volume-title': 'the extended building block was obtained in low yields', 'author': 'Due'} / the extended building block was obtained in low yields by Due

Dates

Type	When
Created	23 years ago (July 26, 2002, 1:15 a.m.)
Deposited	3 years, 11 months ago (Sept. 23, 2021, 4:31 a.m.)
Indexed	1 year, 9 months ago (Oct. 28, 2023, 9:32 a.m.)
Issued	28 years ago (Aug. 1, 1997)
Published	28 years ago (Aug. 1, 1997)
Published Online	27 years, 11 months ago (Aug. 25, 1997)
Published Print	28 years ago (Aug. 1, 1997)

Funders 0

None

BibTeX

@article{Newkome_1997, title={Synthesis and Chemistry of Novel Dendritic Macromolecules Possessing Internal Electroactive Anthraquinonoid Moieties}, volume={30}, ISSN={1520-5835}, url={http://dx.doi.org/10.1021/ma9703214}, DOI={10.1021/ma9703214}, number={17}, journal={Macromolecules}, publisher={American Chemical Society (ACS)}, author={Newkome, George R. and Narayanan, Venkatraj V. and Echegoyen, Luis and Pérez-Cordero, Eduardo and Luftmann, Heinrich}, year={1997}, month=aug, pages={5187–5191} }

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      "key": "ma9703214b00023/ma9703214b00023_1",
      "unstructured": "6:\u2009 80%, mp 140\u2212142 \u00b0C; IR (KBr) 3400 (OH, broad), 1700 (CO) cm-1;13C NMR (DMSO-d6) \u03b4 21.2 (CH2CH2CH2), 29.2, 30.7 (CH2CH2CO2), 35.1, 37.2 (CH2CH2CH2), 45.5 (4\u00b0Ccore), 56.4 (NHC4\u00b0), 68.0, 69.9 (CH2OCH2), 116.0, 127.7, 132.1, 134.5, 137.1, 137.3 (CAr), 170.3, 171.5, 171.7 (CONH), 174.7 (CO2H), 185.5 (COquin); MALDI-TOF-MSm/z2704 (M + Na). Anal. Calcd for C133H144N12O48:\u2009 C, 59.64; H, 5.42; N, 6.27. Found:\u2009 C, 59.42; H, 5.28; N, 6.09."
    },
    {
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      "doi-asserted-by": "crossref",
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    {
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      "volume-title": "bright orange solid, mp 65\u221269 \u00b0C"
    },
    {
      "key": "ma9703214b00027/ma9703214b00027_1",
      "unstructured": "Cyclic voltammograms at 20 \u00b0C were recorded on a BAS-100-W electrochemical apparatus from Bioanalytical systems, Inc. A conventional three-electrode configuration was used with a 3 mm diameter glassy-carbon disk as the working electrode, a platinum working electrode, and a silver wire pseudo-reference electrode. Electrochemical grade (TBA)PF6was recrystallized (EtOH, 2\u00d7) and pulverized. HPLC grade MeCN was dried (P4O10) and vapor transferred directly into the electrochemical cell after three freeze\u2212pump\u2212thaw degassing cycles at 10-5\u221210-6mm Hg. In general, a 0.5 mL sample solution containing 1 mM metal complex and 100 mM (TBA)PF6was prepared by drying the solid reagents directly in the electrochemical cell at 10-5\u221210-6mm Hg and then transferring the solvent directly into it through the vacuum line. Micromolar solutions of1,3, and5\u22128were made in THF and UV spectra obtained on a HP 8452 diode-array spectrophotometer."
    },
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