DOI: 10.1021/ja044959o. Zero Thermal Expansion in a Prussian Blue Analogue

Zero Thermal Expansion in a Prussian Blue Analogue

10.1021/ja044959o

Crossref journal-article

American Chemical Society (ACS)

Journal of the American Chemical Society (316)

Bibliography

Margadonna, S., Prassides, K., & Fitch, A. N. (2004). Zero Thermal Expansion in a Prussian Blue Analogue. Journal of the American Chemical Society, 126(47), 15390â15391.

Authors 3

Serena Margadonna (first)
Kosmas Prassides (additional)
Andrew N. Fitch (additional)

References 15 Referenced 285

{'key': 'ja044959ob00001/ja044959ob00001_1', 'first-page': '3326', 'volume': '3317', 'author': 'Evans J. S. O.', 'year': '1999', 'journal-title': 'J. Chem. Soc., Dalton Trans.'} / J. Chem. Soc., Dalton Trans. by Evans J. S. O. (1999)
10.1107/S0108768194004933 / Acta Crystallogr. B by Rottger K. (1994)
{'key': 'ja044959ob00003/ja044959ob00003_1', 'first-page': '1073', 'volume': '78', 'author': 'Dove M. T.', 'year': '1997', 'journal-title': 'Phys. Rev. Lett.'} / Phys. Rev. Lett. by Dove M. T. (1997)
10.1126/science.272.5258.92 / Science by Mary T. A. (1996)
10.1103/PhysRevLett.31.700 / Phys. Rev. Lett. by Jayaraman A. (1973)
10.1038/nature01994 / Nature by Arvanitidis J. (2003)
{'key': 'ja044959ob00007/ja044959ob00007_1', 'first-page': '81', 'volume': '19', 'author': 'Roy R.', 'year': '1989', 'journal-title': 'Annu. Rev. Mater. Sci.'} / Annu. Rev. Mater. Sci. by Roy R. (1989)
10.1038/nature02011 / Nature by Salvador J. R. (2003)
Fe[Co(CN)6] was prepared as a light yellow solid by reaction of aqueous solutions of FeCl3(0.1 M) and K3[Co(CN)6] (0.1 M), and its stoichiometry was checked by elemental analysis (Fe:Co:H2O = 1.07:1:1.4, K < 10 ppm). X-ray powder diffraction measurements with a STOE diffractometer were consistent with a single-phase material. For the synchrotron X-ray diffraction measurements, the sample was sealed in a thin-wall glass capillary 0.5 mm in diameter. With the sample inside a continuous-flow cryostat, synchrotron X-ray powder diffraction data (λ = 0.85028 Å, 2θ = 5−35°, step size = 0.002°) were collected at various temperatures between 300 and 4.2 K using the high-resolution powder X-ray diffraction beamline ID31 at the ESRF, Grenoble, France. Complementary higher-statistics diffraction data over a longerQ-range were also collected at 300 K using X-rays with λ = 0.42966 Å (2θ = 2.5−25°, step size = 0.002°). Data analysis was performed with the GSAS suite of Rietveld analysis programs (Larsen, A. C.; von Dreele, R. B. GSAS software, LANL Report No. LAUR 86-748).
10.1021/ic50177a008 / Inorg. Chem. by Buser H. J. (1977)
10.1006/jssc.1997.7571 / J. Solid State Chem. by Williams D. J. (1997)
{'key': 'ja044959ob00014/ja044959ob00014_1', 'first-page': '48', 'volume': '173', 'author': 'Tao J. Z.', 'year': '2003', 'journal-title': 'J. Solid State Chem.'} / J. Solid State Chem. by Tao J. Z. (2003)
10.1038/378701a0 / Nature by Ferlay S. (1995)
10.1126/science.272.5262.704 / Science by Sato O. (1996)
Margadonna, S.; Prassides, K.; Fitch, A. N.Angew. Chem.2004, in press.

Dates

Type	When
Created	18 years, 2 months ago (May 30, 2007, 7:26 a.m.)
Deposited	3 years, 10 months ago (Oct. 18, 2021, 7:30 p.m.)
Indexed	2 weeks, 6 days ago (Aug. 6, 2025, 8:58 a.m.)
Issued	20 years, 9 months ago (Nov. 6, 2004)
Published	20 years, 9 months ago (Nov. 6, 2004)
Published Online	20 years, 9 months ago (Nov. 6, 2004)
Published Print	20 years, 8 months ago (Dec. 1, 2004)

Funders 0

None

BibTeX

@article{Margadonna_2004, title={Zero Thermal Expansion in a Prussian Blue Analogue}, volume={126}, ISSN={1520-5126}, url={http://dx.doi.org/10.1021/ja044959o}, DOI={10.1021/ja044959o}, number={47}, journal={Journal of the American Chemical Society}, publisher={American Chemical Society (ACS)}, author={Margadonna, Serena and Prassides, Kosmas and Fitch, Andrew N.}, year={2004}, month=nov, pages={15390–15391} }

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