DOI: 10.1021/ic801677y. Pillared Porphyrin Homologous Series: Intergrowth in Metal−Organic Frameworks

Pillared Porphyrin Homologous Series: Intergrowth in Metal−Organic Frameworks

10.1021/ic801677y

Crossref journal-article

American Chemical Society (ACS)

Inorganic Chemistry (316)

Bibliography

Choi, E.-Y., Barron, P. M., Novotny, R. W., Son, H.-T., Hu, C., & Choe, W. (2008). Pillared Porphyrin Homologous Series: Intergrowth in MetalâOrganic Frameworks. Inorganic Chemistry, 48(2), 426â428.

Authors 6

Eun-Young Choi (first)
Paul M. Barron (additional)
Richard W. Novotny (additional)
Hyun-Tak Son (additional)
Chunhua Hu (additional)
Wonyoung Choe (additional)

References 52 Referenced 177

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aPPF-3.5,10,15,20-Tetrakis(4-carboxyl)-21H,23H-porphine (7.9 mg, 0.01 mmol), cobalt nitrate hexahydrate (8.7 mg, 0.03 mmol), and bpy (3.1 mg, 0.02 mmol) were added to a mixture of DMF (1.5 mL) and ethanol (0.5 mL) in a small capped vial and heated to 80 °C for 24 h, followed by slow cooling to room temperature over 9 h. Yield: 10.4 mg (82% based on porphyrin). Anal. Calcd for [C68H40N8O8Co3]NO3·7H2O·14DMF: C, 53.2; H, 6.2; N, 13.0. Found: C, 53.0; H, 6.2; N, 13.0.
bPPF-4.5,10,15,20-Tetrakis(4-carboxyl)-21H,23H-porphine (7.9 mg, 0.01 mmol), zinc nitrate hexahydrate (8.2 mg, 0.03 mmol), and bpy (3.3 mg, 0.02 mmol) were added to a mixture of DEF (1.5 mL) and ethanol (0.5 mL) in a small capped vial and heated to 80 °C for 24 h, followed by slow cooling to room temperature over 9 h. Yield: 9.0 mg (74% based on porphyrin). Anal. Calcd for C63H36N7O8Zn3·3.7H2O: C, 59.0; H, 3.4; N, 7.7. Found: C, 58.9; H, 3.4; N, 7.9.
cPPF-5.Palladium(II) 5,10,15,20-tetrakis(4-carboxyl)porphine (9.2 mg, 0.01 mmol), cobalt nitrate hexahydrate (8.8mg, 0.03 mmol), and bpy (2.8 mg, 0.02 mmol) were added to a mixture of DEF (1.5 mL) and ethanol (0.5 mL) in a small capped vial and heated to 80 °C for 24 h, followed by slow cooling to room temperature over 9 h. Yield: 8.8 mg (70% based on porphyrin). Anal. Calcd for C58H32N6O8Co2Pd·2CH3CH2OH: C, 60.2; H, 3.6; N, 6.5. Found: C, 59.2; H, 3.5; N, 6.7.
aPPF-3: C68H40N9O11Co3, tetragonal,I4/mmm(No. 139),a= 16.6007(2) Å,c= 24.6892(5) Å,V= 6803.93(18) Å3,Z= 2, R1 = 0.0801, wR2 = 0.2432 (I> 2σ, after SQUEEZE).
bPPF-4: C63H36N7O8Zn3, tetragonal,I4/mmm(No. 139),a= 16.7122(2) Å,c= 54.2436(14) Å,V= 15150.1(5) Å3,Z= 4, R1 = 0.0332, wR2 = 0.0854 (I> 2σ, after SQUEEZE).
cPPF-5: C58H32N6O8Co2Pd, tetragonal,I4/mmm(No. 139),a= 16.7123(1) Å,c= 13.9165(2) Å,V= 3889.89(6) Å3,Z= 1, R1 = 0.0305, wR2 = 0.0836 (I> 2σ, after SQUEEZE).
See theSupporting Information.
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Dates

Type	When
Created	16 years, 8 months ago (Dec. 17, 2008, 9:28 a.m.)
Deposited	2 years, 5 months ago (March 5, 2023, 10:39 a.m.)
Indexed	2 weeks, 6 days ago (Aug. 1, 2025, 11:50 p.m.)
Issued	16 years, 8 months ago (Dec. 17, 2008)
Published	16 years, 8 months ago (Dec. 17, 2008)
Published Online	16 years, 8 months ago (Dec. 17, 2008)
Published Print	16 years, 7 months ago (Jan. 19, 2009)

Funders 0

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BibTeX

@article{Choi_2008, title={Pillared Porphyrin Homologous Series: Intergrowth in Metal−Organic Frameworks}, volume={48}, ISSN={1520-510X}, url={http://dx.doi.org/10.1021/ic801677y}, DOI={10.1021/ic801677y}, number={2}, journal={Inorganic Chemistry}, publisher={American Chemical Society (ACS)}, author={Choi, Eun-Young and Barron, Paul M. and Novotny, Richard W. and Son, Hyun-Tak and Hu, Chunhua and Choe, Wonyoung}, year={2008}, month=dec, pages={426–428} }

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    {
      "key": "ref10/cit10a",
      "unstructured": "aPPF-3.5,10,15,20-Tetrakis(4-carboxyl)-21H,23H-porphine (7.9 mg, 0.01 mmol), cobalt nitrate hexahydrate (8.7 mg, 0.03 mmol), and bpy (3.1 mg, 0.02 mmol) were added to a mixture of DMF (1.5 mL) and ethanol (0.5 mL) in a small capped vial and heated to 80 \u00b0C for 24 h, followed by slow cooling to room temperature over 9 h. Yield: 10.4 mg (82% based on porphyrin). Anal. Calcd for [C68H40N8O8Co3]NO3\u00b77H2O\u00b714DMF: C, 53.2; H, 6.2; N, 13.0. Found: C, 53.0; H, 6.2; N, 13.0."
    },
    {
      "key": "ref10/cit10b",
      "unstructured": "bPPF-4.5,10,15,20-Tetrakis(4-carboxyl)-21H,23H-porphine (7.9 mg, 0.01 mmol), zinc nitrate hexahydrate (8.2 mg, 0.03 mmol), and bpy (3.3 mg, 0.02 mmol) were added to a mixture of DEF (1.5 mL) and ethanol (0.5 mL) in a small capped vial and heated to 80 \u00b0C for 24 h, followed by slow cooling to room temperature over 9 h. Yield: 9.0 mg (74% based on porphyrin). Anal. Calcd for C63H36N7O8Zn3\u00b73.7H2O: C, 59.0; H, 3.4; N, 7.7. Found: C, 58.9; H, 3.4; N, 7.9."
    },
    {
      "key": "ref10/cit10c",
      "unstructured": "cPPF-5.Palladium(II) 5,10,15,20-tetrakis(4-carboxyl)porphine (9.2 mg, 0.01 mmol), cobalt nitrate hexahydrate (8.8mg, 0.03 mmol), and bpy (2.8 mg, 0.02 mmol) were added to a mixture of DEF (1.5 mL) and ethanol (0.5 mL) in a small capped vial and heated to 80 \u00b0C for 24 h, followed by slow cooling to room temperature over 9 h. Yield: 8.8 mg (70% based on porphyrin). Anal. Calcd for C58H32N6O8Co2Pd\u00b72CH3CH2OH: C, 60.2; H, 3.6; N, 6.5. Found: C, 59.2; H, 3.5; N, 6.7."
    },
    {
      "key": "ref11/cit11a",
      "unstructured": "aPPF-3: C68H40N9O11Co3, tetragonal,I4/mmm(No. 139),a= 16.6007(2) \u00c5,c= 24.6892(5) \u00c5,V= 6803.93(18) \u00c53,Z= 2, R1 = 0.0801, wR2 = 0.2432 (I> 2\u03c3, after SQUEEZE)."
    },
    {
      "key": "ref11/cit11b",
      "unstructured": "bPPF-4: C63H36N7O8Zn3, tetragonal,I4/mmm(No. 139),a= 16.7122(2) \u00c5,c= 54.2436(14) \u00c5,V= 15150.1(5) \u00c53,Z= 4, R1 = 0.0332, wR2 = 0.0854 (I> 2\u03c3, after SQUEEZE)."
    },
    {
      "key": "ref11/cit11c",
      "unstructured": "cPPF-5: C58H32N6O8Co2Pd, tetragonal,I4/mmm(No. 139),a= 16.7123(1) \u00c5,c= 13.9165(2) \u00c5,V= 3889.89(6) \u00c53,Z= 1, R1 = 0.0305, wR2 = 0.0836 (I> 2\u03c3, after SQUEEZE)."
    },
    {
      "key": "ref12/cit12",
      "unstructured": "See theSupporting Information."
    },
    {
      "key": "ref13/cit13",
      "doi-asserted-by": "crossref",
      "first-page": "7696",
      "DOI": "10.1021/ic050858v",
      "volume": "44",
      "author": "Kleij A. W.",
      "year": "2005",
      "journal-title": "Inorg. Chem."
    },
    {
      "key": "ref14/cit14a",
      "doi-asserted-by": "crossref",
      "first-page": "11734",
      "DOI": "10.1021/ja063538z",
      "volume": "128",
      "author": "Ma S.",
      "year": "2006",
      "journal-title": "J. Am. Chem. Soc."
    },
    {
      "key": "ref14/cit14b",
      "doi-asserted-by": "crossref",
      "first-page": "9376",
      "DOI": "10.1021/ja0523082",
      "volume": "127",
      "author": "Din\u010da M.",
      "year": "2005",
      "journal-title": "J. Am. Chem. Soc."
    },
    {
      "key": "ref14/cit14c",
      "doi-asserted-by": "crossref",
      "first-page": "8904",
      "DOI": "10.1021/ja061716i",
      "volume": "128",
      "author": "Din\u010da M.",
      "year": "2006",
      "journal-title": "J. Am. Chem. Soc."
    },
    {
      "key": "ref14/cit14d",
      "doi-asserted-by": "crossref",
      "first-page": "1419",
      "DOI": "10.1002/anie.200604362",
      "volume": "46",
      "author": "Din\u010da M.",
      "year": "2007",
      "journal-title": "Angew. Chem., Int. Ed."
    },
    {
      "key": "ref14/cit14e",
      "doi-asserted-by": "crossref",
      "first-page": "16876",
      "DOI": "10.1021/ja0656853",
      "volume": "128",
      "author": "Din\u010da M.",
      "year": "2006",
      "journal-title": "J. Am. Chem. Soc."
    },
    {
      "key": "ref15/cit15",
      "doi-asserted-by": "crossref",
      "first-page": "16846",
      "DOI": "10.1021/ja0649217",
      "volume": "128",
      "author": "Forster P. M.",
      "year": "2006",
      "journal-title": "J. Am. Chem. Soc."
    }
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    "date-parts": [
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    "date-time": "2023-03-05T15:39:23Z",
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        2008,
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