DOI: 10.1021/ic8003855. 3D Metal−Organic Frameworks Based on Elongated Tetracarboxylate Building Blocks for Hydrogen Storage

3D Metal−Organic Frameworks Based on Elongated Tetracarboxylate Building Blocks for Hydrogen Storage

10.1021/ic8003855

Crossref journal-article

American Chemical Society (ACS)

Inorganic Chemistry (316)

Bibliography

Ma, L., Lee, J. Y., Li, J., & Lin, W. (2008). 3D MetalâOrganic Frameworks Based on Elongated Tetracarboxylate Building Blocks for Hydrogen Storage. Inorganic Chemistry, 47(10), 3955â3957.

Authors 4

Liqing Ma (first)
Jeong Yong Lee (additional)
Jing Li (additional)
Wenbin Lin (additional)

References 29 Referenced 81

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All single-crystal X-ray diffraction data were measured at 296 K on a Bruker SMART Apex II CCD-based X-ray diffractometer system equipped with a Mo-target X-ray tube (λ = 0.710 73 Å). Crystal data for5: monoclinic, space groupC2/c,a= 41.483(7) Å,b= 41.783(7) Å,c= 30.968(7) Å, α = 90°, β = 109.895(11)°, γ = 90°,V= 50 472(16) Å3,Z= 8, ρcalcd= 0.462 g/cm3, μ(Mo Kα) = 0.357 mm−1. Data/restraints/parameters: 24 765/866/874, R1 [I> 2σ(I)] = 0.0703, wR2 = 0.1654, R1 (all data) = 0.1634, wR2 (all data) = 0.1774, GOF = 0.707 (0.702 restrained). Crystal data for6: monoclinic, space groupC2/c,a= 41.812(2) Å,b= 41.815(2) Å,c= 31.156(2) Å, α = 90°, β = 109.607(3)°, γ = 90°,V= 51 314(4) Å3,Z= 8, ρcalcd= 0.456 g/cm3, μ(Mo Kα) = 0.394 mm−1. Data/restraints/parameters: 25 746/1014/884, R1 [I > 2σ(I)] = 0.0547, wR2 = 0.1481, R1 (all data) = 0.1043, wR2 (all data) = 0.1519, GOF = 0.973 (0.966 restrained).
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10.1002/anie.200461625 / Angew. Chem., Int. Ed. by Natarajan R. (2005)
The powder X-ray diffraction patterns of evacuated5and6have shown significant peak broadening (Figure S4 in the Supporting Information), but the diffraction peaks of5are sharper than those of6. This result is consistent with the higher framework stability of5.

Dates

Type	When
Created	17 years, 4 months ago (April 17, 2008, 1 a.m.)
Deposited	2 years, 6 months ago (March 5, 2023, 8:48 p.m.)
Indexed	1 month, 2 weeks ago (July 23, 2025, 8:28 a.m.)
Issued	17 years, 4 months ago (April 17, 2008)
Published	17 years, 4 months ago (April 17, 2008)
Published Online	17 years, 4 months ago (April 17, 2008)
Published Print	17 years, 3 months ago (May 19, 2008)

Funders 0

None

BibTeX

@article{Ma_2008, title={3D Metal−Organic Frameworks Based on Elongated Tetracarboxylate Building Blocks for Hydrogen Storage}, volume={47}, ISSN={1520-510X}, url={http://dx.doi.org/10.1021/ic8003855}, DOI={10.1021/ic8003855}, number={10}, journal={Inorganic Chemistry}, publisher={American Chemical Society (ACS)}, author={Ma, Liqing and Lee, Jeong Yong and Li, Jing and Lin, Wenbin}, year={2008}, month=apr, pages={3955–3957} }

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      "unstructured": "All single-crystal X-ray diffraction data were measured at 296 K on a Bruker SMART Apex II CCD-based X-ray diffractometer system equipped with a Mo-target X-ray tube (\u03bb = 0.710\u200973 \u00c5). Crystal data for5: monoclinic, space groupC2/c,a= 41.483(7) \u00c5,b= 41.783(7) \u00c5,c= 30.968(7) \u00c5, \u03b1 = 90\u00b0, \u03b2 = 109.895(11)\u00b0, \u03b3 = 90\u00b0,V= 50\u2009472(16) \u00c53,Z= 8, \u03c1calcd= 0.462 g/cm3, \u03bc(Mo K\u03b1) = 0.357 mm\u22121. Data/restraints/parameters: 24\u2009765/866/874, R1 [I> 2\u03c3(I)] = 0.0703, wR2 = 0.1654, R1 (all data) = 0.1634, wR2 (all data) = 0.1774, GOF = 0.707 (0.702 restrained). Crystal data for6: monoclinic, space groupC2/c,a= 41.812(2) \u00c5,b= 41.815(2) \u00c5,c= 31.156(2) \u00c5, \u03b1 = 90\u00b0, \u03b2 = 109.607(3)\u00b0, \u03b3 = 90\u00b0,V= 51\u2009314(4) \u00c53,Z= 8, \u03c1calcd= 0.456 g/cm3, \u03bc(Mo K\u03b1) = 0.394 mm\u22121. Data/restraints/parameters: 25\u2009746/1014/884, R1 [I > 2\u03c3(I)] = 0.0547, wR2 = 0.1481, R1 (all data) = 0.1043, wR2 (all data) = 0.1519, GOF = 0.973 (0.966 restrained)."
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