DOI: 10.1021/cm802981m. Rapid Microwave Synthesis and Purification of Porous Covalent Organic Frameworks

Rapid Microwave Synthesis and Purification of Porous Covalent Organic Frameworks

10.1021/cm802981m

Crossref journal-article

American Chemical Society (ACS)

Chemistry of Materials (316)

Bibliography

Campbell, N. L., Clowes, R., Ritchie, L. K., & Cooper, A. I. (2009). Rapid Microwave Synthesis and Purification of Porous Covalent Organic Frameworks. Chemistry of Materials, 21(2), 204â206.

Authors 4

Neil L. Campbell (first)
Rob Clowes (additional)
Lyndsey K. Ritchie (additional)
Andrew I. Cooper (additional)

References 24 Referenced 424

10.1038/nature01650 / Nature by Yaghi O. M. (2003)
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10.1021/ja8010176 / J. Am. Chem. Soc. by Jiang J-X. (2008)
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SBETcan vary with the relative pressure range chosen for the calculation. We determined two other values as follows: (i)P/Po= 0.05−0.2;SBET= 2234 m2g−1; correlation coefficient = 0.991; (ii)P/Po= 0.05−0.3;SBET= 1945 m2g−1; correlation coefficient = 0.993. We report hereSBETcalculated over the same relative pressure range used to characterize COF-5 (ref3), which does also give rise to the highest correlation coefficient (0.998).
It is not clear that all of the solvothermal syntheses reported for COF (and MOF) materials actually require the full reaction time that is specified. This highlights an additional advantage of this particular microwave reaction system; that is, the ability to continuously observe the contents of the reactor (Figure1) and to ascertain whether or not a product has formed.
10.1002/adma.200800030 / Adv. Mater. by Tilford R. W. (2008)
10.1021/cm061177g / Chem. Mater. by Tilford R. W. (2006)

Dates

Type	When
Created	16 years, 8 months ago (Jan. 5, 2009, 10:04 a.m.)
Deposited	2 years, 5 months ago (March 15, 2023, 7:06 a.m.)
Indexed	1 day, 7 hours ago (Sept. 4, 2025, 10:32 a.m.)
Issued	16 years, 8 months ago (Jan. 5, 2009)
Published	16 years, 8 months ago (Jan. 5, 2009)
Published Online	16 years, 8 months ago (Jan. 5, 2009)
Published Print	16 years, 7 months ago (Jan. 27, 2009)

Funders 0

None

BibTeX

@article{Campbell_2009, title={Rapid Microwave Synthesis and Purification of Porous Covalent Organic Frameworks}, volume={21}, ISSN={1520-5002}, url={http://dx.doi.org/10.1021/cm802981m}, DOI={10.1021/cm802981m}, number={2}, journal={Chemistry of Materials}, publisher={American Chemical Society (ACS)}, author={Campbell, Neil L. and Clowes, Rob and Ritchie, Lyndsey K. and Cooper, Andrew I.}, year={2009}, month=jan, pages={204–206} }

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