DOI: 10.1021/cm025572s. An Exceptionally Stable Metal−Organic Framework Constructed from the Zn<sub>8</sub>(SiO<sub>4</sub>) Core

An Exceptionally Stable Metal−Organic Framework Constructed from the Zn8(SiO4) Core

10.1021/cm025572s

Crossref journal-article

American Chemical Society (ACS)

Chemistry of Materials (316)

Bibliography

Yang, S. Y., Long, L. S., Jiang, Y. B., Huang, R. B., & Zheng, L. S. (2002). An Exceptionally Stable MetalâOrganic Framework Constructed from the Zn8(SiO4) Core. Chemistry of Materials, 14(8), 3229â3231.

Authors 5

S. Y. Yang (first)
L. S. Long (additional)
Y. B. Jiang (additional)
R. B. Huang (additional)
L. S. Zheng (additional)

References 36 Referenced 110

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Terephthalic acid [p-C6H4(COOH)2; 0.33 g, 2.0 mmol], Na2SiO3·9H2O (0.06 g, 0.2 mmol), and NaOH (0.16 g, 4 mmol) were dissolved in 35 mL of water, and 1 mol/L HNO3was added drop by drop to pH ∼ 7. Then to the above solution was added Zn(NO3)2·6H2O (0.59 g, 2.0 mmol). Finally 10 mL of ethylene glycol was added. The suspension was heated to 180 °C at the rate of 2.5 °C/h, and the resulting solution was kept at 180 °C for 100 h and then cooled to room temperature at the rate of 5 °C/h. This gave colorless cuboid crystals of the compound (0.09 g, yield 28% based on Na2SiO3·9H2O). Elem anal. Calcd for C48H24O28SiZn8: C, 36.04; H, 1.51. Found: C, 36.06; H, 1.54. FT-IR (KBr pellet): 2926(w), 1635(w), 1597(s), 1506, 1439, 1399(vs), 1319(w), 1290(w), 1161(w), 1107(w), 1019, 950, 881(w), 824, 739, 617, 562 cm-1. TGA performed on a polycrystalline sample under a flow of air showed no weight loss below ca. 500 °C. Further heating of the sample from 500 to 800 °C results in the decomposition of the material with a weight loss of 55.34%.
Crystal dimensions 0.36 × 0.32 × 0.29 mm, monoclinic, space groupC(2)/c,a= 19.640(4) Å,b= 14.064(3) Å,c= 19.561(4) Å,β= 90.30(3)°,V= 5403.0(19) Å3,Z= 4,ρcalcd= 1.967 g cm-3, andμ(Mo Kα) = 3.603 mm-1. Of the 5465 reflections measured (1.78 ≤ θ ≤ 25.97°), 5305 symmetry independent reflections were used to solve the structure. Based on all of these data and 370 refined parameters,R1= 0.0376,wR2= 0.0897, and the goodness of fit onF2is 0.986. The maximum and minimum peaks correspond to 0.520 and −0.393 e Å-3, respectively. Crystallographic data reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-174992. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, U.K. (fax, (+44)1223-336-033; e-mail, deposit@ ccdc.cam.ac.uk).
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Dates

Type	When
Created	22 years, 11 months ago (Sept. 17, 2002, 4:41 p.m.)
Deposited	3 years, 10 months ago (Oct. 3, 2021, 2:36 a.m.)
Indexed	1 month, 4 weeks ago (June 23, 2025, 3:28 a.m.)
Issued	23 years, 1 month ago (July 17, 2002)
Published	23 years, 1 month ago (July 17, 2002)
Published Online	23 years, 1 month ago (July 17, 2002)
Published Print	23 years ago (Aug. 1, 2002)

Funders 0

None

BibTeX

@article{Yang_2002, title={An Exceptionally Stable Metalâˆ’Organic Framework Constructed from the Zn8(SiO4) Core}, volume={14}, ISSN={1520-5002}, url={http://dx.doi.org/10.1021/cm025572s}, DOI={10.1021/cm025572s}, number={8}, journal={Chemistry of Materials}, publisher={American Chemical Society (ACS)}, author={Yang, S. Y. and Long, L. S. and Jiang, Y. B. and Huang, R. B. and Zheng, L. S.}, year={2002}, month=jul, pages={3229â€“3231} }

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      "unstructured": "Terephthalic acid [p-C6H4(COOH)2; 0.33 g, 2.0 mmol], Na2SiO3\u00b79H2O (0.06 g, 0.2 mmol), and NaOH (0.16 g, 4 mmol) were dissolved in 35 mL of water, and 1 mol/L HNO3was added drop by drop to pH \u223c 7. Then to the above solution was added Zn(NO3)2\u00b76H2O (0.59 g, 2.0 mmol). Finally 10 mL of ethylene glycol was added. The suspension was heated to 180 \u00b0C at the rate of 2.5 \u00b0C/h, and the resulting solution was kept at 180 \u00b0C for 100 h and then cooled to room temperature at the rate of 5 \u00b0C/h. This gave colorless cuboid crystals of the compound (0.09 g, yield 28% based on Na2SiO3\u00b79H2O). Elem anal. Calcd for C48H24O28SiZn8:\u2009 C, 36.04; H, 1.51. Found:\u2009 C, 36.06; H, 1.54. FT-IR (KBr pellet):\u2009 2926(w), 1635(w), 1597(s), 1506, 1439, 1399(vs), 1319(w), 1290(w), 1161(w), 1107(w), 1019, 950, 881(w), 824, 739, 617, 562 cm-1. TGA performed on a polycrystalline sample under a flow of air showed no weight loss below ca. 500 \u00b0C. Further heating of the sample from 500 to 800 \u00b0C results in the decomposition of the material with a weight loss of 55.34%."
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      "unstructured": "Crystal dimensions 0.36 \u00d7 0.32 \u00d7 0.29 mm, monoclinic, space groupC(2)/c,a= 19.640(4) \u00c5,b= 14.064(3) \u00c5,c= 19.561(4) \u00c5,\u03b2= 90.30(3)\u00b0,V= 5403.0(19) \u00c53,Z= 4,\u03c1calcd= 1.967 g cm-3, and\u03bc(Mo K\u03b1) = 3.603 mm-1. Of the 5465 reflections measured (1.78 \u2264 \u03b8 \u2264 25.97\u00b0), 5305 symmetry independent reflections were used to solve the structure. Based on all of these data and 370 refined parameters,R1= 0.0376,wR2= 0.0897, and the goodness of fit onF2is 0.986. The maximum and minimum peaks correspond to 0.520 and \u22120.393 e \u00c5-3, respectively. Crystallographic data reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-174992. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, U.K. (fax, (+44)1223-336-033; e-mail, deposit@ ccdc.cam.ac.uk)."
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