DOI: 10.1021/cg005508s. Synthesis of Zinc Oxalate Coordination Polymers via Unprecedented Oxidative Coupling of Methanol to Oxalic Acid

Synthesis of Zinc Oxalate Coordination Polymers via Unprecedented Oxidative Coupling of Methanol to Oxalic Acid

10.1021/cg005508s

Crossref journal-article

American Chemical Society (ACS)

Crystal Growth & Design (316)

Bibliography

Evans, O. R., & Lin, W. (2000). Synthesis of Zinc Oxalate Coordination Polymers via Unprecedented Oxidative Coupling of Methanol to Oxalic Acid. Crystal Growth & Design, 1(1), 9â11.

Authors 2

Owen R. Evans (first)
Wenbin Lin (additional)

References 25 Referenced 118

{'key': 'cg005508sb00001/cg005508sb00001_1', 'first-page': '288', 'volume': '283', 'author': 'Zaworotko M.', 'year': '1994', 'journal-title': 'J. Chem. Soc. Rev.'} / J. Chem. Soc. Rev. by Zaworotko M. (1994)
{'key': 'cg005508sb00002/cg005508sb00002_1', 'first-page': '2684', 'volume': '38', 'author': 'Hagrman P. J.', 'year': '1999', 'journal-title': 'Angew. Chem., Int. Ed.'} / Angew. Chem., Int. Ed. by Hagrman P. J. (1999)
10.1002/(SICI)1521-3773(19980619)37:11<1460::AID-ANIE1460>3.0.CO;2-Z / Angew. Chem., Int. Ed. Engl. by Batten S. R. (1998)
10.1021/ar970151f / Acc. Chem. Res. by Yaghi O. M. (1998)
10.1002/anie.199714311 / Angew. Chem., Int. Ed. Engl. by Janiak C. (1997)
{'key': 'cg005508sb00006/cg005508sb00006_1', 'first-page': '304', 'volume': '46', 'author': 'Munakata M.', 'year': '1999', 'journal-title': 'Adv. Inorg. Chem.'} / Adv. Inorg. Chem. by Munakata M. (1999)
10.1126/science.283.5405.1150 / Science by Chui S. S.-Y. (1999)
{'key': 'cg005508sb00008/cg005508sb00008_1', 'first-page': '8215', 'volume': '121', 'author': 'Kiang Y.-H.', 'year': '1999', 'journal-title': 'J. Am. Chem. Soc.'} / J. Am. Chem. Soc. by Kiang Y.-H. (1999)
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10.1126/science.271.5245.49 / Science by Sato O. (1996)
{'key': 'cg005508sb00012/cg005508sb00012_1', 'first-page': '48', 'volume': '279', 'author': 'Kahn O.', 'year': '1998', 'journal-title': 'J. Science'} / J. Science by Kahn O. (1998)
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10.1002/(SICI)1521-3773(19990215)38:4<538::AID-ANIE538>3.0.CO;2-W / Angew. Chem., Int. Ed. by Evans O. R. (1999)
{'key': 'cg005508sb00015/cg005508sb00015_1', 'first-page': '13273', 'volume': '120', 'author': 'Lin W.', 'year': '1998', 'journal-title': 'J. Am. Chem. Soc.'} / J. Am. Chem. Soc. by Lin W. (1998)
{'key': 'cg005508sb00016/cg005508sb00016_1', 'first-page': '11250', 'volume': '121', 'author': 'Lin W.', 'year': '1999', 'journal-title': 'J. Am. Chem. Soc.'} / J. Am. Chem. Soc. by Lin W. (1999)
{'key': 'cg005508sb00018/cg005508sb00018_1', 'first-page': '1754', 'volume': '38', 'author': 'Shan Y. K.', 'year': '1999', 'journal-title': 'Angew. Chem., Int. Ed.'} / Angew. Chem., Int. Ed. by Shan Y. K. (1999)
{'key': 'cg005508sb00019/cg005508sb00019_1', 'first-page': '2704', 'volume': '38', 'author': 'Lu J. Y.', 'year': '1999', 'journal-title': 'Inorg. Chem.'} / Inorg. Chem. by Lu J. Y. (1999)
{'key': 'cg005508sb00020/cg005508sb00020_1', 'first-page': '1753', 'volume': '121', 'author': 'Ranganathan A.', 'year': '1999', 'journal-title': 'J. Am. Chem. Soc.'} / J. Am. Chem. Soc. by Ranganathan A. (1999)
A mixture of Zn(NO3)2·6H2O (0.50 mmol, 0.1485 g), pyridine (0.3 mL), and ethanol (0.5 mL) was thoroughly mixed in a heavy-walled Pyrex tube. The Pyrex tube was sealed under vacuum and heated at 140 °C. Colorless platelike crystals and brown powders of zincite were obtained after 14 days. Yield for1: 0.018 g (11.6%). Yield for zincite: 0.017 g (41.9%). IR for1(cm-1, KBr): 3107 (w), 1676 (s), 1610 (s), 1449 (s), 1316 (m), 1219 (w), 1159 (w), 796 (m) 795 (m), 702 (m), 629 (w). Thermal analysis: 1exhibits a 48.3% weight loss by 230 °C corresponding to a loss of two pyridine molecules per formula unit (calcd 50.8%).
A mixture of Zn(NO3)2·6H2O (0.50 mmol, 0.1485 g), pyridine (0.3 mL), and methanol (0.5 mL) was thoroughly mixed in a heavy-walled Pyrex tube. The Pyrex tube was sealed under vacuum and heated at 140 °C. Colorless platelike crystals and brown powders of zincite were obtained after 5 days. Yield for2: 0.013 g (8.9%). Yield for zincite: 0.009 g (22.1%). IR for2(cm-1, KBr): 3065 (m), 1615 (s), 1362 (w), 1313 (s), 1183 (w), 769 (s), 773 (m), 682 (s), 493 (w). Thermal analysis: 2exhibits no weight loss until 430 °C.
{'key': 'cg005508sb00024/cg005508sb00024_1', 'first-page': '635', 'volume-title': 'H. P.', 'year': '1974', 'edition': '2'} / H. P. (1974)
{'key': 'cg005508sb00027/cg005508sb00027_1', 'first-page': '505', 'volume': '8', 'author': 'The', 'year': '1979', 'journal-title': 'Struct. Commun.'} / Struct. Commun. by The (1979)
10.1021/cm990434x / Chem. Mater. by Vaidhyanathan R. (1999)
10.1021/ic00108a001 / Inorg. Chem. by Farrell R. P. (1995)

Dates

Type	When
Created	23 years ago (July 26, 2002, 12:52 a.m.)
Deposited	2 years, 5 months ago (March 5, 2023, 12:12 p.m.)
Indexed	2 days, 14 hours ago (Aug. 21, 2025, 12:57 p.m.)
Issued	24 years, 9 months ago (Nov. 1, 2000)
Published	24 years, 9 months ago (Nov. 1, 2000)
Published Online	24 years, 9 months ago (Nov. 1, 2000)
Published Print	24 years, 7 months ago (Jan. 1, 2001)

Funders 0

None

BibTeX

@article{Evans_2000, title={Synthesis of Zinc Oxalate Coordination Polymers via Unprecedented Oxidative Coupling of Methanol to Oxalic Acid}, volume={1}, ISSN={1528-7505}, url={http://dx.doi.org/10.1021/cg005508s}, DOI={10.1021/cg005508s}, number={1}, journal={Crystal Growth & Design}, publisher={American Chemical Society (ACS)}, author={Evans, Owen R. and Lin, Wenbin}, year={2000}, month=nov, pages={9–11} }

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