DOI: 10.1016/s0378-5173(03)00339-9. Structural properties of magnesium stearate pseudopolymorphs: effect of temperature

Structural properties of magnesium stearate pseudopolymorphs: effect of temperature

10.1016/s0378-5173(03)00339-9

Crossref journal-article

Elsevier BV

International Journal of Pharmaceutics (78)

Bibliography

Bracconi, P., AndrÃ¨s, C., & Ndiaye, A. (2003). Structural properties of magnesium stearate pseudopolymorphs: effect of temperature. International Journal of Pharmaceutics, 262(1â2), 109â124.

Authors 3

Pierre Bracconi (first)
Cyrille Andrès (additional)
Augustin Ndiaye (additional)

References 23 Referenced 29

American Society for Testing and Materials, 1965. Powder diffraction file, file 5-0292.
10.1016/S0378-5173(01)00624-X / Int. J. Pharm. / On the difficulty of assessing the specific surface area of magnesium stearate by Andrès (2001)
10.3109/03639049609065947 / Drug Dev. Ind. Pharm. / Influence of the physicochemical variability of magnesium stearate on its lubricant properties: possible solutions by Barra (1996)
10.3109/03639048909052521 / Drug Dev. Ind. Pharm. / Raw materials by Brittain (1989)
10.1002/jps.2600770715 / J. Pharm. Sci. / Chemical, physical and lubricant properties of magnesium stearate by Ertel (1988)
European Pharmacopeia, 2002. Magnesium stearate. Direction Européenne de la Qualité des Médicaments, 4th ed. pp. 1647–1649.
10.1002/jps.2600811214 / Pharm. Sci. / Physical and lubrication properties of magnesium stearate by Leinonen (1992)
10.1016/0025-5408(93)90065-L / Mat. Res. Bull. / Synchrotron high resolution powder study of molecular packing in hydrate calcium stearate by Lelann (1993)
10.1016/0378-5173(88)90281-5 / Int. J. Pharm. / Structure-lubricity evaluation of magnesium stearate by Marwaha (1988)
Müller, B.W., 1977a. The pseudo-polymorphism of magnesium stearate. In: First International Conference on Pharmacy Technology, Paris, May 31–June 2, pp. 134–141.
{'key': '10.1016/S0378-5173(03)00339-9_BIB11', 'first-page': '161', 'article-title': 'Tribologische Gesetzmässigkeiten und Erkenntnisse in der Tablettentechnologie. 3: Untersuchungen an reinen Magnesium- und Calciumstearaten', 'volume': '39', 'author': 'Müller', 'year': '1977', 'journal-title': 'Pharm. Ind.'} / Pharm. Ind. / Tribologische Gesetzmässigkeiten und Erkenntnisse in der Tablettentechnologie. 3: Untersuchungen an reinen Magnesium- und Calciumstearaten by Müller (1977)
10.1002/ardp.19773100903 / Arch. Pharm. / Die Pseudo-Polymorphie von Magnesiumsalzen höherer Fettsäuren by Müller (1977)
{'key': '10.1016/S0378-5173(03)00339-9_BIB13', 'first-page': '729', 'article-title': 'Tribologische Gesetzmässigkeiten und Erkenntnisse in der Tablettentechnologie. 6: Einflüsse physikalisher Eigenschaften chemisch reiner Magnesiumstearate auf die Schmiereigenshaften bei der Tablettierung', 'volume': '44', 'author': 'Müller', 'year': '1982', 'journal-title': 'Pharm. Ind.'} / Pharm. Ind. / Tribologische Gesetzmässigkeiten und Erkenntnisse in der Tablettentechnologie. 6: Einflüsse physikalisher Eigenschaften chemisch reiner Magnesiumstearate auf die Schmiereigenshaften bei der Tablettierung by Müller (1982)
10.1016/0040-6031(94)01950-L / Thermochim. Acta / The effect of moisture on the structure of magnesium stearate by Rajala (1995)
10.1098/rspa.1925.0102 / Proc. Roy. Soc. Lond. A / On the distribution of intensity in the X-ray spectra of certain long-chain organic compounds by Schearer (1925)
10.1007/BF02272348 / Struct. Chem. / Physical characterization of the polymorphic variations of magnesium stearate and magnesium palmitate hydrate species by Sharpe (1997)
Small, D.M., 1986. Handbook of Lipid Research. The Physical Chemistry of Lipids. Plenum Press, New York. (10.1007/978-1-4899-5333-9)
{'key': '10.1016/S0378-5173(03)00339-9_BIB18', 'first-page': '2199', 'article-title': 'Structure des phases mésopmorphes du stéarate de calcium anhydre', 'volume': '251', 'author': 'Spegt', 'year': '1960', 'journal-title': 'CR Acad. Sci. Paris'} / CR Acad. Sci. Paris / Structure des phases mésopmorphes du stéarate de calcium anhydre by Spegt (1960)
{'key': '10.1016/S0378-5173(03)00339-9_BIB19', 'first-page': '4316', 'article-title': 'Structure des phases mésomorphes du stéarate de magnésium', 'volume': '254', 'author': 'Spegt', 'year': '1962', 'journal-title': 'CR Acad. Sci. Paris'} / CR Acad. Sci. Paris / Structure des phases mésomorphes du stéarate de magnésium by Spegt (1962)
10.1107/S0365110X64000494 / Acta Cryst. / La structure des colloı̈des d’association. X. description de la structure des savons de calcium à température ordinaire et à température élevée by Spegt (1964)
10.1107/S0365110X48000302 / Acta Cryst. / Indexing method of powder photographs of long-spacing compounds by Vand (1948)
10.1107/S0365110X48000806 / Acta Cryst. / A third graphical method of indexing powder photographs of long-spacing compounds by Vand (1948)
10.1021/ie50478a056 / Ind. Eng. Chem. / Characterisation of heavy metal soaps by X-ray diffraction by Vold (1949)

Dates

Type	When
Created	22 years ago (Aug. 7, 2003, 6:13 p.m.)
Deposited	6 years, 5 months ago (March 14, 2019, 7:55 p.m.)
Indexed	3 months, 3 weeks ago (May 8, 2025, 4:25 p.m.)
Issued	22 years, 1 month ago (Aug. 1, 2003)
Published	22 years, 1 month ago (Aug. 1, 2003)
Published Print	22 years, 1 month ago (Aug. 1, 2003)

Funders 0

None

BibTeX

@article{Bracconi_2003, title={Structural properties of magnesium stearate pseudopolymorphs: effect of temperature}, volume={262}, ISSN={0378-5173}, url={http://dx.doi.org/10.1016/s0378-5173(03)00339-9}, DOI={10.1016/s0378-5173(03)00339-9}, number={1–2}, journal={International Journal of Pharmaceutics}, publisher={Elsevier BV}, author={Bracconi, Pierre and Andrès, Cyrille and Ndiaye, Augustin}, year={2003}, month=aug, pages={109–124} }

JSON

{
  "indexed": {
    "date-parts": [
      [
        2025,
        5,
        8
      ]
    ],
    "date-time": "2025-05-08T20:25:35Z",
    "timestamp": 1746735935573
  },
  "reference-count": 23,
  "publisher": "Elsevier BV",
  "issue": "1-2",
  "license": [
    {
      "start": {
        "date-parts": [
          [
            2003,
            8,
            1
          ]
        ],
        "date-time": "2003-08-01T00:00:00Z",
        "timestamp": 1059696000000
      },
      "content-version": "tdm",
      "delay-in-days": 0,
      "URL": "https://www.elsevier.com/tdm/userlicense/1.0/"
    }
  ],
  "content-domain": {
    "domain": [],
    "crossmark-restriction": false
  },
  "published-print": {
    "date-parts": [
      [
        2003,
        8
      ]
    ]
  },
  "DOI": "10.1016/s0378-5173(03)00339-9",
  "type": "journal-article",
  "created": {
    "date-parts": [
      [
        2003,
        8,
        7
      ]
    ],
    "date-time": "2003-08-07T22:13:29Z",
    "timestamp": 1060294409000
  },
  "page": "109-124",
  "source": "Crossref",
  "is-referenced-by-count": 29,
  "title": "Structural properties of magnesium stearate pseudopolymorphs: effect of temperature",
  "prefix": "10.1016",
  "volume": "262",
  "author": [
    {
      "given": "Pierre",
      "family": "Bracconi",
      "sequence": "first",
      "affiliation": []
    },
    {
      "given": "Cyrille",
      "family": "Andr\u00e8s",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "Augustin",
      "family": "Ndiaye",
      "sequence": "additional",
      "affiliation": []
    }
  ],
  "member": "78",
  "reference": [
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB1",
      "unstructured": "American Society for Testing and Materials, 1965. Powder diffraction file, file 5-0292."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB2",
      "doi-asserted-by": "crossref",
      "first-page": "153",
      "DOI": "10.1016/S0378-5173(01)00624-X",
      "article-title": "On the difficulty of assessing the specific surface area of magnesium stearate",
      "volume": "218",
      "author": "Andr\u00e8s",
      "year": "2001",
      "journal-title": "Int. J. Pharm."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB3",
      "doi-asserted-by": "crossref",
      "first-page": "1105",
      "DOI": "10.3109/03639049609065947",
      "article-title": "Influence of the physicochemical variability of magnesium stearate on its lubricant properties: possible solutions",
      "volume": "22",
      "author": "Barra",
      "year": "1996",
      "journal-title": "Drug Dev. Ind. Pharm."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB4",
      "doi-asserted-by": "crossref",
      "first-page": "2083",
      "DOI": "10.3109/03639048909052521",
      "article-title": "Raw materials",
      "volume": "15",
      "author": "Brittain",
      "year": "1989",
      "journal-title": "Drug Dev. Ind. Pharm."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB5",
      "doi-asserted-by": "crossref",
      "first-page": "625",
      "DOI": "10.1002/jps.2600770715",
      "article-title": "Chemical, physical and lubricant properties of magnesium stearate",
      "volume": "77",
      "author": "Ertel",
      "year": "1988",
      "journal-title": "J. Pharm. Sci."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB6",
      "unstructured": "European Pharmacopeia, 2002. Magnesium stearate. Direction Europ\u00e9enne de la Qualit\u00e9 des M\u00e9dicaments, 4th ed. pp. 1647\u20131649."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB7",
      "doi-asserted-by": "crossref",
      "first-page": "1194",
      "DOI": "10.1002/jps.2600811214",
      "article-title": "Physical and lubrication properties of magnesium stearate",
      "volume": "81",
      "author": "Leinonen",
      "year": "1992",
      "journal-title": "Pharm. Sci."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB8",
      "doi-asserted-by": "crossref",
      "first-page": "329",
      "DOI": "10.1016/0025-5408(93)90065-L",
      "article-title": "Synchrotron high resolution powder study of molecular packing in hydrate calcium stearate",
      "volume": "28",
      "author": "Lelann",
      "year": "1993",
      "journal-title": "Mat. Res. Bull."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB9",
      "doi-asserted-by": "crossref",
      "first-page": "249",
      "DOI": "10.1016/0378-5173(88)90281-5",
      "article-title": "Structure-lubricity evaluation of magnesium stearate",
      "volume": "43",
      "author": "Marwaha",
      "year": "1988",
      "journal-title": "Int. J. Pharm."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB10",
      "unstructured": "M\u00fcller, B.W., 1977a. The pseudo-polymorphism of magnesium stearate. In: First International Conference on Pharmacy Technology, Paris, May 31\u2013June 2, pp. 134\u2013141."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB11",
      "first-page": "161",
      "article-title": "Tribologische Gesetzm\u00e4ssigkeiten und Erkenntnisse in der Tablettentechnologie. 3: Untersuchungen an reinen Magnesium- und Calciumstearaten",
      "volume": "39",
      "author": "M\u00fcller",
      "year": "1977",
      "journal-title": "Pharm. Ind."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB12",
      "doi-asserted-by": "crossref",
      "first-page": "693",
      "DOI": "10.1002/ardp.19773100903",
      "article-title": "Die Pseudo-Polymorphie von Magnesiumsalzen h\u00f6herer Fetts\u00e4uren",
      "volume": "310",
      "author": "M\u00fcller",
      "year": "1977",
      "journal-title": "Arch. Pharm."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB13",
      "first-page": "729",
      "article-title": "Tribologische Gesetzm\u00e4ssigkeiten und Erkenntnisse in der Tablettentechnologie. 6: Einfl\u00fcsse physikalisher Eigenschaften chemisch reiner Magnesiumstearate auf die Schmiereigenshaften bei der Tablettierung",
      "volume": "44",
      "author": "M\u00fcller",
      "year": "1982",
      "journal-title": "Pharm. Ind."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB14",
      "doi-asserted-by": "crossref",
      "first-page": "177",
      "DOI": "10.1016/0040-6031(94)01950-L",
      "article-title": "The effect of moisture on the structure of magnesium stearate",
      "volume": "248",
      "author": "Rajala",
      "year": "1995",
      "journal-title": "Thermochim. Acta"
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB15",
      "doi-asserted-by": "crossref",
      "first-page": "655",
      "DOI": "10.1098/rspa.1925.0102",
      "article-title": "On the distribution of intensity in the X-ray spectra of certain long-chain organic compounds",
      "volume": "108",
      "author": "Schearer",
      "year": "1925",
      "journal-title": "Proc. Roy. Soc. Lond. A"
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB16",
      "doi-asserted-by": "crossref",
      "first-page": "73",
      "DOI": "10.1007/BF02272348",
      "article-title": "Physical characterization of the polymorphic variations of magnesium stearate and magnesium palmitate hydrate species",
      "volume": "8",
      "author": "Sharpe",
      "year": "1997",
      "journal-title": "Struct. Chem."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB17",
      "doi-asserted-by": "crossref",
      "unstructured": "Small, D.M., 1986. Handbook of Lipid Research. The Physical Chemistry of Lipids. Plenum Press, New York.",
      "DOI": "10.1007/978-1-4899-5333-9"
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB18",
      "first-page": "2199",
      "article-title": "Structure des phases m\u00e9sopmorphes du st\u00e9arate de calcium anhydre",
      "volume": "251",
      "author": "Spegt",
      "year": "1960",
      "journal-title": "CR Acad. Sci. Paris"
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB19",
      "first-page": "4316",
      "article-title": "Structure des phases m\u00e9somorphes du st\u00e9arate de magn\u00e9sium",
      "volume": "254",
      "author": "Spegt",
      "year": "1962",
      "journal-title": "CR Acad. Sci. Paris"
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB20",
      "doi-asserted-by": "crossref",
      "first-page": "198",
      "DOI": "10.1107/S0365110X64000494",
      "article-title": "La structure des collo\u0131\u0308des d\u2019association. X. description de la structure des savons de calcium \u00e0 temp\u00e9rature ordinaire et \u00e0 temp\u00e9rature \u00e9lev\u00e9e",
      "volume": "17",
      "author": "Spegt",
      "year": "1964",
      "journal-title": "Acta Cryst."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB21",
      "doi-asserted-by": "crossref",
      "first-page": "109",
      "DOI": "10.1107/S0365110X48000302",
      "article-title": "Indexing method of powder photographs of long-spacing compounds",
      "volume": "1",
      "author": "Vand",
      "year": "1948",
      "journal-title": "Acta Cryst."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB22",
      "doi-asserted-by": "crossref",
      "first-page": "290",
      "DOI": "10.1107/S0365110X48000806",
      "article-title": "A third graphical method of indexing powder photographs of long-spacing compounds",
      "volume": "1",
      "author": "Vand",
      "year": "1948",
      "journal-title": "Acta Cryst."
    },
    {
      "key": "10.1016/S0378-5173(03)00339-9_BIB23",
      "doi-asserted-by": "crossref",
      "first-page": "2311",
      "DOI": "10.1021/ie50478a056",
      "article-title": "Characterisation of heavy metal soaps by X-ray diffraction",
      "volume": "41",
      "author": "Vold",
      "year": "1949",
      "journal-title": "Ind. Eng. Chem."
    }
  ],
  "container-title": "International Journal of Pharmaceutics",
  "original-title": [],
  "language": "en",
  "link": [
    {
      "URL": "https://api.elsevier.com/content/article/PII:S0378517303003399?httpAccept=text/xml",
      "content-type": "text/xml",
      "content-version": "vor",
      "intended-application": "text-mining"
    },
    {
      "URL": "https://api.elsevier.com/content/article/PII:S0378517303003399?httpAccept=text/plain",
      "content-type": "text/plain",
      "content-version": "vor",
      "intended-application": "text-mining"
    }
  ],
  "deposited": {
    "date-parts": [
      [
        2019,
        3,
        14
      ]
    ],
    "date-time": "2019-03-14T23:55:46Z",
    "timestamp": 1552607746000
  },
  "score": 1,
  "resource": {
    "primary": {
      "URL": "https://linkinghub.elsevier.com/retrieve/pii/S0378517303003399"
    }
  },
  "subtitle": [],
  "short-title": [],
  "issued": {
    "date-parts": [
      [
        2003,
        8
      ]
    ]
  },
  "references-count": 23,
  "journal-issue": {
    "issue": "1-2",
    "published-print": {
      "date-parts": [
        [
          2003,
          8
        ]
      ]
    }
  },
  "alternative-id": [
    "S0378517303003399"
  ],
  "URL": "http://dx.doi.org/10.1016/S0378-5173(03)00339-9",
  "relation": {},
  "ISSN": [
    "0378-5173"
  ],
  "subject": [],
  "container-title-short": "International Journal of Pharmaceutics",
  "published": {
    "date-parts": [
      [
        2003,
        8
      ]
    ]
  }
}