DOI: 10.1007/bf02655157. The preparation of C<sub>19</sub> dicarboxylic acid by the koch reaction

The preparation of C19 dicarboxylic acid by the koch reaction

10.1007/bf02655157

Crossref journal-article

Wiley

Journal of the American Oil Chemists' Society (311)

Abstract

Abstract and SummaryThis paper describes the preparation of C19 dicarboxylic acid by the Koch reaction with carbon monoxide and sulfuric acid of oleic, tall oil fatty, and partially hydrogenated tall oil fatty acids. The effects of changing reaction conditions upon the yield and purity of the product were examined. With the best conditions, it was possible to prepare light‐colored, heat‐stable C19 dicarboxylic acid in 83% overall weight yield at 96% purity, containing 75% tertiary isomers and 25% secondary.

Bibliography

Lawson, N. E., Cheng, T. T., & Slezak, F. B. (1977). The preparation of C19 dicarboxylic acid by the koch reaction. Journal of the American Oil Chemistsâ Society, 54(6), 215â218. Portico.

Authors 3

N. E. Lawson (first)
T. T. Cheng (additional)
F. B. Slezak (additional)

References 13 Referenced 10

{'key': 'e_1_2_1_2_1', 'first-page': '234', 'volume': '31', 'author': 'Sreenivasan B.', 'year': '1966', 'journal-title': 'Indian Oil Soap J.'} / Indian Oil Soap J. by Sreenivasan B. (1966)
10.1007/BF02672546
Ward B.F. U.S. Patent 3 753 968 (1973).
10.1007/BF02886865
{'key': 'e_1_2_1_6_1', 'first-page': '451', 'volume': '49', 'author': 'Pryde E.H.', 'year': '1972', 'journal-title': 'Ibid.'} / Ibid. by Pryde E.H. (1972)
10.1007/978-3-642-85857-4
Miller E.J. andA.Mais U.S. Pat 3 481 977 (1969).
Kirkpatrick E.C. U.S. Pat. 2 372 090 (1945). (10.1136/bmj.2.4419.372)
10.1007/BF02632093
10.1246/nikkashi1898.71.8_1179
10.1007/BF02633595
Reppe W. N.vonKutepow andH.Detzer Ger. Pat. 1 006 849 (1957).
10.1007/978-3-642-85857-4

Dates

Type	When
Created	18 years, 1 month ago (July 16, 2007, 7:51 p.m.)
Deposited	1 year, 11 months ago (Sept. 28, 2023, 4:16 a.m.)
Indexed	1 year, 10 months ago (Sept. 29, 2023, 1:40 a.m.)
Issued	48 years, 2 months ago (June 1, 1977)
Published	48 years, 2 months ago (June 1, 1977)
Published Online	48 years, 2 months ago (June 1, 1977)
Published Print	48 years, 2 months ago (June 1, 1977)

Funders 0

None

BibTeX

@article{Lawson_1977, title={The preparation of C19 dicarboxylic acid by the koch reaction}, volume={54}, ISSN={1558-9331}, url={http://dx.doi.org/10.1007/bf02655157}, DOI={10.1007/bf02655157}, number={6}, journal={Journal of the American Oil Chemists’ Society}, publisher={Wiley}, author={Lawson, N. E. and Cheng, T. T. and Slezak, F. B.}, year={1977}, month=jun, pages={215–218} }

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