DOI: 10.1002/sia.1695. Conventional and tomographic atom probe investigations of secondary‐hardening carbides

Conventional and tomographic atom probe investigations of secondary‐hardening carbides

10.1002/sia.1695

Crossref journal-article

Wiley

Surface and Interface Analysis (311)

Abstract

AbstractSecondary‐hardening carbides in high‐speed steels are very important microstructural constituents responsible for the excellent properties of these steels in cutting applications, therefore detailed knowledge about their precipitation reactions and coarsening behaviour is of great interest.The investigations were carried out on steel grades HS2‐10‐1‐8 and HS6‐5‐2 with nominal chemical compositions (in wt.%) of 1.1C–3.9Cr–1.4W–9.2Mo–1.2V–8Co (HS2‐10‐1‐8) and 0.9C–4.1Cr–6.4W–5Mo–1.8V (HS6‐5‐2). The austenitizing temperatures for HS2‐10‐1‐8 and HS6‐5‐2 were 1190°C and 1210°C, respectively. After quenching, the samples were heated non‐isothermally from room temperature to different final temperatures at 15 K min−1. The resulting precipitates were analysed to determine composition, size and morphology using both a conventional one‐dimensional atom probe and a three‐dimensional tomographic atom probe. The results obtained by both techniques from samples at different heat treatment conditions are compared. Owing to the different evaporation field of the precipitates, an overlap of the ion trajectories from matrix and precipitates can be observed. Methods to correct the analytical results are discussed. Copyright © 2004 John Wiley & Sons, Ltd.

Bibliography

Leitner, H., Stiller, K., Andren, H., & Danoix, F. (2004). Conventional and tomographic atom probe investigations of secondaryâhardening carbides. Surface and Interface Analysis, 36(5â6), 540â545. Portico.

Authors 4

H. Leitner (first)
K. Stiller (additional)
H‐O. Andren (additional)
F. Danoix (additional)

References 14 Referenced 20

{'volume-title': 'Steels', 'year': '1995', 'author': 'Honeycombe RWK', 'key': 'e_1_2_1_2_2'} / Steels by Honeycombe RWK (1995)
10.1016/0001-6160(84)90218-9
{'key': 'e_1_2_1_4_2', 'first-page': '223', 'volume': '171', 'author': 'Kuo K', 'year': '1953', 'journal-title': 'J. Iron Steel Inst.'} / J. Iron Steel Inst. by Kuo K (1953)
10.1016/0001-6160(84)90092-0
10.1016/0001-6160(88)90136-8
{'key': 'e_1_2_1_7_2', 'first-page': '405', 'volume': '48', 'author': 'Stiller K', 'year': '1987', 'journal-title': 'J. Phys.'} / J. Phys. by Stiller K (1987)
10.1016/0956-7151(92)90116-V
{'key': 'e_1_2_1_9_2', 'first-page': '386', 'volume': '83', 'author': 'Karagöz S', 'year': '1992', 'journal-title': 'Z. Metallkd.'} / Z. Metallkd. by Karagöz S (1992)
10.1007/BF02804359
{'volume-title': 'Atom Probe Microanalysis–Principles and Applications to Materials Problems', 'year': '1989', 'author': 'Miller MK', 'key': 'e_1_2_1_11_2'} / Atom Probe Microanalysis–Principles and Applications to Materials Problems by Miller MK (1989)
{'key': 'e_1_2_1_12_2', 'first-page': '1', 'volume': '64', 'author': 'Baker RG', 'year': '1959', 'journal-title': 'ISI Spec. Rep'} / ISI Spec. Rep by Baker RG (1959)
10.1002/srin.195803018
GustafsonA.PhD Thesis KTH Stockholm Stockholm 2000.
{'key': 'e_1_2_1_15_2', 'first-page': '571', 'volume': '47', 'author': 'Blavette D', 'year': '1987', 'journal-title': 'J. Phys.'} / J. Phys. by Blavette D (1987)

Dates

Type	When
Created	21 years, 2 months ago (June 2, 2004, 7:01 a.m.)
Deposited	1 year, 11 months ago (Sept. 1, 2023, 1:39 p.m.)
Indexed	3 months ago (May 21, 2025, 5:09 p.m.)
Issued	21 years, 3 months ago (May 1, 2004)
Published	21 years, 3 months ago (May 1, 2004)
Published Online	21 years, 2 months ago (June 2, 2004)
Published Print	21 years, 3 months ago (May 1, 2004)

Funders 0

None

BibTeX

@article{Leitner_2004, title={Conventional and tomographic atom probe investigations of secondary‐hardening carbides}, volume={36}, ISSN={1096-9918}, url={http://dx.doi.org/10.1002/sia.1695}, DOI={10.1002/sia.1695}, number={5–6}, journal={Surface and Interface Analysis}, publisher={Wiley}, author={Leitner, H. and Stiller, K. and Andren, H‐O. and Danoix, F.}, year={2004}, month=may, pages={540–545} }

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