DOI: 10.1002/jccs.198500004. Photochemical Reaction of Decacarbonyldirhenium with Thiophene and Crystal Structure of Tetradecacarbonylhydridotrirhenium

Photochemical Reaction of Decacarbonyldirhenium with Thiophene and Crystal Structure of Tetradecacarbonylhydridotrirhenium

10.1002/jccs.198500004

Crossref journal-article

Wiley

Journal of the Chinese Chemical Society (311)

Abstract

AbstractThe photochemical reaction of Re2(CO)10 with thiophene in hexane solution was investigated under vacuum. Three rhenium clusters: H2Re3(CO)12, HRe3(CO)14 and Re3(CO)14(OH)4, were isolated. The structure of Fellmann‐Kaesz cluster Complex HRe3(CO)14 was determined by use of the X‐ray diffraction method. The three rhenium atoms form a plane of symmetry and L: Re1Re2Re3 is 107°. The ten carbonyl groups bonded to the two terminal rhenium atoms Re1 and Re3, are staggered with respect to the central rhenium atoms. The bond lengths are 3.10 Å for Re2‐Re3 and 3.34 Å for Re1‐Re2. The bridging hydride is between Re1 and Re2.

Bibliography

Yang, C. S., Cheng, C. P., Guo, L. W., & Wang, Y. (1985). Photochemical Reaction of Decacarbonyldirhenium with Thiophene and Crystal Structure of Tetradecacarbonylhydridotrirhenium. Journal of the Chinese Chemical Society, 32(1), 17â22. Portico.

Authors 4

C.S. Yang (first)
C.P. Cheng (additional)
L.W. Guo (additional)
Y. Wang (additional)

References 22 Referenced 10

10.1021/ja01027a052
10.1021/ja01076a024
10.1016/0020-1650(66)80094-6
10.1021/ja01032a038
{'key': 'e_1_2_1_6_2', 'first-page': '6374', 'article-title': 'J. Am. Chem. Soc.', 'volume': '89', 'author': 'Bau R.', 'year': '1967', 'journal-title': 'Inorg. Chew.'} / Inorg. Chew. / J. Am. Chem. Soc. by Bau R. (1967)
10.1016/S0022-328X(00)96153-9
10.1016/S0022-328X(00)83555-X
10.1016/S0022-328X(00)93741-0
10.1021/ja00431a079
10.1016/S0022-328X(00)82416-X
10.1016/S0022-328X(00)92288-5
10.1021/ic50112a022
10.1021/ja00844a079
{'key': 'e_1_2_1_15_2', 'first-page': '700', 'article-title': 'Angew. Chem. Int. Ed. Engl.', 'volume': '14', 'author': 'Herberhold M.', 'year': '1975', 'journal-title': 'J. Am. Chem. Sec'} / J. Am. Chem. Sec / Angew. Chem. Int. Ed. Engl. by Herberhold M. (1975)
{'key': 'e_1_2_1_16_2', 'first-page': '1143', 'volume': '1', 'author': 'Gard D.R.', 'year': '1982', 'journal-title': 'Org.'} / Org. by Gard D.R. (1982)
10.1021/ja00382a041
{'key': 'e_1_2_1_18_2', 'first-page': '1750', 'article-title': 'J. Chem. Phys.', 'volume': '23', 'author': 'Dahl L.F.', 'year': '1957', 'journal-title': 'Inorg., Chem.'} / Inorg., Chem. / J. Chem. Phys. by Dahl L.F. (1957)
{'key': 'e_1_2_1_19_2', 'volume-title': 'Metal Cluster Compound', 'author': 'Johnson B.F.G.', 'year': '1980'} / Metal Cluster Compound by Johnson B.F.G. (1980)
10.1021/ja00728a014
{'key': 'e_1_2_1_21_2', 'first-page': '344', 'article-title': 'Bond Length Data Quoted', 'volume': '9', 'author': 'Kaesz H.D.', 'year': '1973', 'journal-title': 'Chem. Brit.'} / Chem. Brit. / Bond Length Data Quoted by Kaesz H.D. (1973)
10.1016/S0022-328X(00)87272-1
10.1021/ja00987a071

Dates

Type	When
Created	10 years, 3 months ago (June 4, 2015, 11:38 a.m.)
Deposited	1 year, 10 months ago (Oct. 16, 2023, 2:13 a.m.)
Indexed	1 year, 10 months ago (Oct. 17, 2023, 1:11 a.m.)
Issued	40 years, 6 months ago (March 1, 1985)
Published	40 years, 6 months ago (March 1, 1985)
Published Online	11 years, 11 months ago (Sept. 24, 2013)
Published Print	40 years, 6 months ago (March 1, 1985)

Funders 0

None

BibTeX

@article{Yang_1985, title={Photochemical Reaction of Decacarbonyldirhenium with Thiophene and Crystal Structure of Tetradecacarbonylhydridotrirhenium}, volume={32}, ISSN={2192-6549}, url={http://dx.doi.org/10.1002/jccs.198500004}, DOI={10.1002/jccs.198500004}, number={1}, journal={Journal of the Chinese Chemical Society}, publisher={Wiley}, author={Yang, C.S. and Cheng, C.P. and Guo, L.W. and Wang, Y.}, year={1985}, month=mar, pages={17–22} }

JSON

{
  "indexed": {
    "date-parts": [
      [
        2023,
        10,
        17
      ]
    ],
    "date-time": "2023-10-17T05:11:02Z",
    "timestamp": 1697519462627
  },
  "reference-count": 22,
  "publisher": "Wiley",
  "issue": "1",
  "license": [
    {
      "start": {
        "date-parts": [
          [
            2013,
            9,
            24
          ]
        ],
        "date-time": "2013-09-24T00:00:00Z",
        "timestamp": 1379980800000
      },
      "content-version": "vor",
      "delay-in-days": 10434,
      "URL": "http://onlinelibrary.wiley.com/termsAndConditions#vor"
    }
  ],
  "content-domain": {
    "domain": [],
    "crossmark-restriction": false
  },
  "published-print": {
    "date-parts": [
      [
        1985,
        3
      ]
    ]
  },
  "abstract": "<jats:title>Abstract</jats:title><jats:p>The photochemical reaction of Re<jats:sub>2</jats:sub>(CO)<jats:sub>10</jats:sub> with thiophene in hexane solution was investigated under vacuum. Three rhenium clusters: H<jats:sub>2</jats:sub>Re<jats:sub>3</jats:sub>(CO)<jats:sub>12</jats:sub>, HRe<jats:sub>3</jats:sub>(CO)<jats:sub>14</jats:sub> and Re<jats:sub>3</jats:sub>(CO)<jats:sub>14</jats:sub>(OH)<jats:sub>4</jats:sub>, were isolated. The structure of Fellmann\u2010Kaesz cluster Complex HRe<jats:sub>3</jats:sub>(CO)<jats:sub>14</jats:sub> was determined by use of the X\u2010ray diffraction method. The three rhenium atoms form a plane of symmetry and L: Re<jats:sub>1</jats:sub>Re<jats:sub>2</jats:sub>Re<jats:sub>3</jats:sub> is 107\u00b0. The ten carbonyl groups bonded to the two terminal rhenium atoms Re<jats:sub>1</jats:sub> and Re<jats:sub>3</jats:sub>, are staggered with respect to the central rhenium atoms. The bond lengths are 3.10 \u00c5 for Re<jats:sub>2</jats:sub>\u2010Re<jats:sub>3</jats:sub> and 3.34 \u00c5 for Re<jats:sub>1</jats:sub>\u2010Re<jats:sub>2</jats:sub>. The bridging hydride is between Re<jats:sub>1</jats:sub> and Re<jats:sub>2</jats:sub>.</jats:p>",
  "DOI": "10.1002/jccs.198500004",
  "type": "journal-article",
  "created": {
    "date-parts": [
      [
        2015,
        6,
        4
      ]
    ],
    "date-time": "2015-06-04T15:38:08Z",
    "timestamp": 1433432288000
  },
  "page": "17-22",
  "source": "Crossref",
  "is-referenced-by-count": 10,
  "title": "Photochemical Reaction of Decacarbonyldirhenium with Thiophene and Crystal Structure of Tetradecacarbonylhydridotrirhenium",
  "prefix": "10.1002",
  "volume": "32",
  "author": [
    {
      "given": "C.S.",
      "family": "Yang",
      "sequence": "first",
      "affiliation": []
    },
    {
      "given": "C.P.",
      "family": "Cheng",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "L.W.",
      "family": "Guo",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "Y.",
      "family": "Wang",
      "sequence": "additional",
      "affiliation": []
    }
  ],
  "member": "311",
  "published-online": {
    "date-parts": [
      [
        2013,
        9,
        24
      ]
    ]
  },
  "reference": [
    {
      "key": "e_1_2_1_2_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja01027a052"
    },
    {
      "key": "e_1_2_1_3_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja01076a024"
    },
    {
      "key": "e_1_2_1_4_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/0020-1650(66)80094-6"
    },
    {
      "key": "e_1_2_1_5_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja01032a038"
    },
    {
      "key": "e_1_2_1_6_2",
      "first-page": "6374",
      "article-title": "J. Am. Chem. Soc.",
      "volume": "89",
      "author": "Bau R.",
      "year": "1967",
      "journal-title": "Inorg. Chew."
    },
    {
      "key": "e_1_2_1_7_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/S0022-328X(00)96153-9"
    },
    {
      "key": "e_1_2_1_8_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/S0022-328X(00)83555-X"
    },
    {
      "key": "e_1_2_1_9_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/S0022-328X(00)93741-0"
    },
    {
      "key": "e_1_2_1_10_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja00431a079"
    },
    {
      "key": "e_1_2_1_11_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/S0022-328X(00)82416-X"
    },
    {
      "key": "e_1_2_1_12_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/S0022-328X(00)92288-5"
    },
    {
      "key": "e_1_2_1_13_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ic50112a022"
    },
    {
      "key": "e_1_2_1_14_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja00844a079"
    },
    {
      "key": "e_1_2_1_15_2",
      "first-page": "700",
      "article-title": "Angew. Chem. Int. Ed. Engl.",
      "volume": "14",
      "author": "Herberhold M.",
      "year": "1975",
      "journal-title": "J. Am. Chem. Sec"
    },
    {
      "key": "e_1_2_1_16_2",
      "first-page": "1143",
      "volume": "1",
      "author": "Gard D.R.",
      "year": "1982",
      "journal-title": "Org."
    },
    {
      "key": "e_1_2_1_17_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja00382a041"
    },
    {
      "key": "e_1_2_1_18_2",
      "first-page": "1750",
      "article-title": "J. Chem. Phys.",
      "volume": "23",
      "author": "Dahl L.F.",
      "year": "1957",
      "journal-title": "Inorg., Chem."
    },
    {
      "key": "e_1_2_1_19_2",
      "volume-title": "Metal Cluster Compound",
      "author": "Johnson B.F.G.",
      "year": "1980"
    },
    {
      "key": "e_1_2_1_20_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja00728a014"
    },
    {
      "key": "e_1_2_1_21_2",
      "first-page": "344",
      "article-title": "Bond Length Data Quoted",
      "volume": "9",
      "author": "Kaesz H.D.",
      "year": "1973",
      "journal-title": "Chem. Brit."
    },
    {
      "key": "e_1_2_1_22_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/S0022-328X(00)87272-1"
    },
    {
      "key": "e_1_2_1_23_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja00987a071"
    }
  ],
  "container-title": "Journal of the Chinese Chemical Society",
  "original-title": [],
  "language": "en",
  "link": [
    {
      "URL": "https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fjccs.198500004",
      "content-type": "unspecified",
      "content-version": "vor",
      "intended-application": "text-mining"
    },
    {
      "URL": "https://onlinelibrary.wiley.com/doi/pdf/10.1002/jccs.198500004",
      "content-type": "unspecified",
      "content-version": "vor",
      "intended-application": "similarity-checking"
    }
  ],
  "deposited": {
    "date-parts": [
      [
        2023,
        10,
        16
      ]
    ],
    "date-time": "2023-10-16T06:13:11Z",
    "timestamp": 1697436791000
  },
  "score": 1,
  "resource": {
    "primary": {
      "URL": "https://onlinelibrary.wiley.com/doi/10.1002/jccs.198500004"
    }
  },
  "subtitle": [],
  "short-title": [],
  "issued": {
    "date-parts": [
      [
        1985,
        3
      ]
    ]
  },
  "references-count": 22,
  "journal-issue": {
    "issue": "1",
    "published-print": {
      "date-parts": [
        [
          1985,
          3
        ]
      ]
    }
  },
  "alternative-id": [
    "10.1002/jccs.198500004"
  ],
  "URL": "http://dx.doi.org/10.1002/jccs.198500004",
  "relation": {},
  "ISSN": [
    "0009-4536",
    "2192-6549"
  ],
  "subject": [],
  "container-title-short": "J Chinese Chemical Soc",
  "published": {
    "date-parts": [
      [
        1985,
        3
      ]
    ]
  }
}