DOI: 10.1002/anie.201003377. Single‐Crystal to Single‐Crystal Cross‐Linking of an Interpenetrating Chiral Metal–Organic Framework and Implications in Asymmetric Catalysis

Single‐Crystal to Single‐Crystal Cross‐Linking of an Interpenetrating Chiral Metal–Organic Framework and Implications in Asymmetric Catalysis

10.1002/anie.201003377

Crossref journal-article

Wiley

Angewandte Chemie International Edition (311)

Bibliography

Ma, L., Wu, C., Wanderley, M. M., & Lin, W. (2010). SingleâCrystal to SingleâCrystal CrossâLinking of an Interpenetrating Chiral MetalâOrganic Framework and Implications in Asymmetric Catalysis. Angewandte Chemie International Edition, 49(44), 8244â8248. Portico.

Authors 4

Liqing Ma (first)
Chuan‐De Wu (additional)
Marcela M. Wanderley (additional)
Wenbin Lin (additional)

References 50 Referenced 160

10.1021/cr9900432
10.1021/ar0001012
10.1039/b200393g
10.1021/ar020022l
10.1126/science.1135445
10.1039/b817360p
10.1002/ange.200801163
10.1002/anie.200801163
10.1038/nature03852
10.1039/b807083k
10.1039/b807080f
10.1002/ange.200805101
10.1002/anie.200805101
10.1002/ange.200804853
10.1002/anie.200804853
10.1021/ja909629f
10.1021/ja803383k
10.1021/ja906198y
10.1038/nmat2608
10.1021/ja052431t
10.1002/ange.200602099
10.1002/anie.200602099
L. Ma J. M. Falkowski C. Abney W. Lin Nat. Chem.2010 DOI:.
The determination of the unit cell and data collections for colorless crystals of1and2were performed on a Siemens SMART CCD diffractometer. Data for Ti‐2was collected on a Bruker SMART APEX II diffractometer. Crystallographic data for1: Orthorhombic space groupI212121 a=13.0884(3) b=28.7131(7) c=42.8771(11) Å V=16 113.6(7) Å3 Z=8 ρcalcd=0.858 g cm−3 μ(MoKα)=0.635 mm−1.R1(I>2σ(I))=0.0713 wR2(I>2σ(I))=0.1513 Flack parameter=0.00(3) and GOF=1.062. Crystallographic data for2: Orthorhombic space groupI212121 a=12.7526(10) b=26.9066(19) c=44.199(3) Å V=15 166(2) Å3 Z=8 ρcalcd=0.861 g cm−3 μ(MoKα)=0.672 mm−1.R1(I>2σ(I))=0.0492 wR2(I>2σ(I))=0.1011 Flack parameter=0.10(1) and GOF=0.890. Crystallographic data for Ti‐2: Orthorhombic space groupI212121 a=13.1451(4) b=31.9683(10) c=39.8933(12) Å V=16 344.0(9) Å3 Z=8 ρcalcd=0.805 g cm−3 μ(CuKα)=1.409 mm−1.R1(I>2σ(I))=0.0956 wR2(I>2σ(I))=0.2442 Flack parameter=0.10(6) and GOF=1.223. CCDC 772189 772190 and 778882 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre viawww.ccdc.cam.ac.uk/data_request/cif.
{'key': 'e_1_2_3_28_2', 'first-page': '453', 'volume': '25', 'author': 'Blatov V. A.', 'year': '1999', 'journal-title': 'Russ. J. Coord. Chem.'} / Russ. J. Coord. Chem. by Blatov V. A. (1999)
10.1107/S0108767392001260
10.1021/ja0276974
10.1002/ange.200903433
10.1002/anie.200903433
10.1021/ja901440g
10.1002/ange.200462711
10.1002/anie.200462711
10.1021/ar700145r
10.1002/chem.200801064
10.1038/nmat2101
Related catalytic reactions have recently been reported for molecular solids see:
10.1002/ange.201000874
10.1002/anie.201000874
10.1038/nature09085
10.1021/cr000411y
The Ti content (Ti/Zn=0.42) determined by the ICP‐MS analysis is slightly higher than that determined from the X‐ray structure (Ti/Zn=0.25) thus suggesting that there might be some disordered unreacted Ti(OiPr)4in the open channels of Ti‐2.

Dates

Type	When
Created	14 years, 11 months ago (Sept. 21, 2010, 6:42 p.m.)
Deposited	1 year, 10 months ago (Oct. 16, 2023, 4:40 a.m.)
Indexed	3 weeks ago (Aug. 2, 2025, 12:41 a.m.)
Issued	14 years, 11 months ago (Sept. 21, 2010)
Published	14 years, 11 months ago (Sept. 21, 2010)
Published Online	14 years, 11 months ago (Sept. 21, 2010)
Published Print	14 years, 9 months ago (Oct. 25, 2010)

Funders 0

None

BibTeX

@article{Ma_2010, title={Single‐Crystal to Single‐Crystal Cross‐Linking of an Interpenetrating Chiral Metal–Organic Framework and Implications in Asymmetric Catalysis}, volume={49}, ISSN={1521-3773}, url={http://dx.doi.org/10.1002/anie.201003377}, DOI={10.1002/anie.201003377}, number={44}, journal={Angewandte Chemie International Edition}, publisher={Wiley}, author={Ma, Liqing and Wu, Chuan‐De and Wanderley, Marcela M. and Lin, Wenbin}, year={2010}, month=sep, pages={8244–8248} }

JSON

{
  "indexed": {
    "date-parts": [
      [
        2025,
        8,
        2
      ]
    ],
    "date-time": "2025-08-02T04:41:03Z",
    "timestamp": 1754109663559
  },
  "reference-count": 50,
  "publisher": "Wiley",
  "issue": "44",
  "license": [
    {
      "start": {
        "date-parts": [
          [
            2010,
            9,
            21
          ]
        ],
        "date-time": "2010-09-21T00:00:00Z",
        "timestamp": 1285027200000
      },
      "content-version": "vor",
      "delay-in-days": 0,
      "URL": "http://onlinelibrary.wiley.com/termsAndConditions#vor"
    }
  ],
  "content-domain": {
    "domain": [],
    "crossmark-restriction": false
  },
  "published-print": {
    "date-parts": [
      [
        2010,
        10,
        25
      ]
    ]
  },
  "DOI": "10.1002/anie.201003377",
  "type": "journal-article",
  "created": {
    "date-parts": [
      [
        2010,
        9,
        21
      ]
    ],
    "date-time": "2010-09-21T22:42:06Z",
    "timestamp": 1285108926000
  },
  "page": "8244-8248",
  "source": "Crossref",
  "is-referenced-by-count": 160,
  "title": "Single\u2010Crystal to Single\u2010Crystal Cross\u2010Linking of an Interpenetrating Chiral Metal\u2013Organic Framework and Implications in Asymmetric Catalysis",
  "prefix": "10.1002",
  "volume": "49",
  "author": [
    {
      "given": "Liqing",
      "family": "Ma",
      "sequence": "first",
      "affiliation": []
    },
    {
      "given": "Chuan\u2010De",
      "family": "Wu",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "Marcela M.",
      "family": "Wanderley",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "Wenbin",
      "family": "Lin",
      "sequence": "additional",
      "affiliation": []
    }
  ],
  "member": "311",
  "published-online": {
    "date-parts": [
      [
        2010,
        9,
        21
      ]
    ]
  },
  "reference": [
    {
      "key": "e_1_2_3_1_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_2_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/cr9900432"
    },
    {
      "key": "e_1_2_3_3_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ar0001012"
    },
    {
      "key": "e_1_2_3_4_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/b200393g"
    },
    {
      "key": "e_1_2_3_5_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ar020022l"
    },
    {
      "key": "e_1_2_3_6_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1126/science.1135445"
    },
    {
      "key": "e_1_2_3_7_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/b817360p"
    },
    {
      "key": "e_1_2_3_8_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_9_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200801163"
    },
    {
      "key": "e_1_2_3_9_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200801163"
    },
    {
      "key": "e_1_2_3_10_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1038/nature03852"
    },
    {
      "key": "e_1_2_3_11_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_12_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/b807083k"
    },
    {
      "key": "e_1_2_3_13_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/b807080f"
    },
    {
      "key": "e_1_2_3_14_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_15_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200805101"
    },
    {
      "key": "e_1_2_3_15_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200805101"
    },
    {
      "key": "e_1_2_3_16_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200804853"
    },
    {
      "key": "e_1_2_3_16_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200804853"
    },
    {
      "key": "e_1_2_3_17_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja909629f"
    },
    {
      "key": "e_1_2_3_18_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_19_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja803383k"
    },
    {
      "key": "e_1_2_3_20_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja906198y"
    },
    {
      "key": "e_1_2_3_21_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1038/nmat2608"
    },
    {
      "key": "e_1_2_3_22_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_23_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja052431t"
    },
    {
      "key": "e_1_2_3_24_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200602099"
    },
    {
      "key": "e_1_2_3_24_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200602099"
    },
    {
      "key": "e_1_2_3_25_2",
      "unstructured": "L. Ma J.\u2005M. Falkowski C. Abney W. Lin Nat. Chem.2010 DOI:."
    },
    {
      "key": "e_1_2_3_26_2",
      "unstructured": "The determination of the unit cell and data collections for colorless crystals of1and2were performed on a Siemens SMART CCD diffractometer. Data for Ti\u20102was collected on a Bruker SMART APEX II diffractometer. Crystallographic data for1: Orthorhombic space groupI212121 a=13.0884(3) b=28.7131(7) c=42.8771(11)\u2005\u00c5 V=16\u2009113.6(7)\u2005\u00c53 Z=8 \u03c1calcd=0.858\u2005g\u2009cm\u22123 \u03bc(MoK\u03b1)=0.635\u2005mm\u22121.R1(I>2\u03c3(I))=0.0713 wR2(I>2\u03c3(I))=0.1513 Flack parameter=0.00(3) and GOF=1.062. Crystallographic data for2: Orthorhombic space groupI212121 a=12.7526(10) b=26.9066(19) c=44.199(3)\u2005\u00c5 V=15\u2009166(2)\u2005\u00c53 Z=8 \u03c1calcd=0.861\u2005g\u2009cm\u22123 \u03bc(MoK\u03b1)=0.672\u2005mm\u22121.R1(I>2\u03c3(I))=0.0492 wR2(I>2\u03c3(I))=0.1011 Flack parameter=0.10(1) and GOF=0.890. Crystallographic data for Ti\u20102: Orthorhombic space groupI212121 a=13.1451(4) b=31.9683(10) c=39.8933(12)\u2005\u00c5 V=16\u2009344.0(9)\u2005\u00c53 Z=8 \u03c1calcd=0.805\u2005g\u2009cm\u22123 \u03bc(CuK\u03b1)=1.409\u2005mm\u22121.R1(I>2\u03c3(I))=0.0956 wR2(I>2\u03c3(I))=0.2442 Flack parameter=0.10(6) and GOF=1.223. CCDC\u2005772189 772190 and 778882 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre viawww.ccdc.cam.ac.uk/data_request/cif."
    },
    {
      "key": "e_1_2_3_27_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_28_2",
      "first-page": "453",
      "volume": "25",
      "author": "Blatov V. A.",
      "year": "1999",
      "journal-title": "Russ. J. Coord. Chem."
    },
    {
      "key": "e_1_2_3_29_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1107/S0108767392001260"
    },
    {
      "key": "e_1_2_3_30_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja0276974"
    },
    {
      "key": "e_1_2_3_31_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_32_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200903433"
    },
    {
      "key": "e_1_2_3_32_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200903433"
    },
    {
      "key": "e_1_2_3_33_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja901440g"
    },
    {
      "key": "e_1_2_3_34_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_35_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200462711"
    },
    {
      "key": "e_1_2_3_35_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200462711"
    },
    {
      "key": "e_1_2_3_36_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ar700145r"
    },
    {
      "key": "e_1_2_3_37_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/chem.200801064"
    },
    {
      "key": "e_1_2_3_38_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1038/nmat2101"
    },
    {
      "key": "e_1_2_3_39_2",
      "unstructured": "Related catalytic reactions have recently been reported for molecular solids see:"
    },
    {
      "key": "e_1_2_3_40_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.201000874"
    },
    {
      "key": "e_1_2_3_40_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.201000874"
    },
    {
      "key": "e_1_2_3_41_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1038/nature09085"
    },
    {
      "key": "e_1_2_3_42_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/cr000411y"
    },
    {
      "key": "e_1_2_3_43_2",
      "unstructured": "The Ti content (Ti/Zn=0.42) determined by the ICP\u2010MS analysis is slightly higher than that determined from the X\u2010ray structure (Ti/Zn=0.25) thus suggesting that there might be some disordered unreacted Ti(OiPr)4in the open channels of Ti\u20102."
    }
  ],
  "container-title": "Angewandte Chemie International Edition",
  "original-title": [],
  "language": "en",
  "link": [
    {
      "URL": "https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fanie.201003377",
      "content-type": "unspecified",
      "content-version": "vor",
      "intended-application": "text-mining"
    },
    {
      "URL": "https://onlinelibrary.wiley.com/doi/pdf/10.1002/anie.201003377",
      "content-type": "unspecified",
      "content-version": "vor",
      "intended-application": "similarity-checking"
    }
  ],
  "deposited": {
    "date-parts": [
      [
        2023,
        10,
        16
      ]
    ],
    "date-time": "2023-10-16T08:40:31Z",
    "timestamp": 1697445631000
  },
  "score": 1,
  "resource": {
    "primary": {
      "URL": "https://onlinelibrary.wiley.com/doi/10.1002/anie.201003377"
    }
  },
  "subtitle": [],
  "short-title": [],
  "issued": {
    "date-parts": [
      [
        2010,
        9,
        21
      ]
    ]
  },
  "references-count": 50,
  "journal-issue": {
    "issue": "44",
    "published-print": {
      "date-parts": [
        [
          2010,
          10,
          25
        ]
      ]
    }
  },
  "alternative-id": [
    "10.1002/anie.201003377"
  ],
  "URL": "http://dx.doi.org/10.1002/anie.201003377",
  "relation": {},
  "ISSN": [
    "1433-7851",
    "1521-3773"
  ],
  "subject": [],
  "container-title-short": "Angew Chem Int Ed",
  "published": {
    "date-parts": [
      [
        2010,
        9,
        21
      ]
    ]
  }
}