Nanoporous Lanthanide–Copper(II) Coordination Polymers: Syntheses and Crystal Structures of [{M2(Cu3(iminodiacetate)6)}⋅8 H2O]n (M=La, Nd, Eu)
10.1002/anie.200390153
Crossref journal-article
Wiley
Angewandte Chemie International Edition (311)
Bibliography

Ren, Y., Long, L., Mao, B., Yuan, Y., Huang, R., & Zheng, L. (2003). Nanoporous Lanthanide–Copper(II) Coordination Polymers: Syntheses and Crystal Structures of [{M2(Cu3(iminodiacetate)6)}⋅8 H2O]n (M=La, Nd, Eu). Angewandte Chemie International Edition, 42(5), 532–535. Portico.

Authors 6
  1. Yan‐Ping Ren (first)
  2. La‐Sheng Long (additional)
  3. Bing‐Wei Mao (additional)
  4. You‐Zhu Yuan (additional)
  5. Rong‐Bin Huang (additional)
  6. Lan‐Sun Zheng (additional)
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  52. X‐ray crystal structure analysis: The data were collected at 293(2) K on a CAD4 diffractometer (MoKαradiation;λ=0.71073 Å). The structure was solved by direct methods (SHELXTL Version 5.10) and refined by full‐matrix least‐squares onF2. All non‐hydrogen atoms were refined anisotropically. Crystal data for [C24H46Cu3La2N6O32]n(1): 0.50×0.40×0.40 mm trigonal space groupP${\bar{3}}$c1 (no. 165) a=13.4713(19) c=14.922(3) Å γ=120° V=2345.3(7) Å3 Z=2 ρcalcd=1.958 g cm−3 μ(MoKα)=3.223 mm−1 MW=1398.98. Of the 2615 reflections measured (2<2θ<56) 1708 symmetry‐independent reflections were used to solve the structure. Based on these data and 108 refined parameters R1=0.0410 (all data) wR2=0.0757 GOF (F2)=1.111. Crystal data for [C24H46Cu3Nd2N6O32]n(2): 0.52×0.40×0.40 mm trigonal space groupP${\bar{3}}$c1 (no. 165) a=13.4027(19) c=14.669(3) Å γ=120° V=2282.0(6) Å3 Z=2 ρcalcd=2.019 g cm−3 μ(MoKα)=3.699 mm−1 MW=1409.64. Of the 1854 reflections measured (2<2θ<56) 1189 symmetry‐independent reflections were used to solve the structure. Based on these data and 114 refined parameters R1=0.0642 (all data) wR2=0.0870 and GOF (F2)=1.011. Crystal data for [C24H46Cu3Eu2N6O32]n(3): 0.33×0.18×0.17 mm trigonal space groupP${\bar{3}}$c1 (no. 165) a=13.306(5) c=14.528(5) Å γ=120° V=2227.6(14) Å3 Z=2 ρcalcd=2.101 g cm−3 μ(MoKα)=4.291 mm−1 MW=1425.08. Of the 1533 reflections measured (2<2θ<56) 1468 symmetry‐independent reflections were used to solve the structure. Based on these data and 107 refined parameters R1=0.0497 (all data) wR2=0.1143 GOF (F2)=1.127. Crystal data for [C24H38Cu3La2N6O29]n(1 a): 0.32×0.24×0.22 mm trigonal space groupP${\bar{3}}$c1 (no. 165) a=13.5588(3) c=14.9986(6) Å γ=120° V=2387.94(12) Å3 Z=2 ρcalcd=1.857 g cm−3 μ(MoKα)=3.157 mm−1 MW=1344.98. Of the 9010 reflections measured (2<2θ<56) 1721 symmetry‐independent reflections were used to solve the structure. Based on these data and 100 refined parameters R1=0.1017 (all data) wR2=0.2352 GOF (F2)=1.155. Crystal data for [C24H38Cu3Eu2N6O29]n(3 a): 0.30×0.22×0.20 mm trigonal space groupP${\bar{3}}$c1 (no. 165) a=13.3031(2) c=14.5660(3) Å γ=120° V=2232.42(7) Å3 Z=2 ρcalcd=2.025 g cm−3 μ(MoKα)=4.273 mm−1 MW=1369.08. Of the 9618 reflections measured (2<2θ<48) 1170 symmetry‐independent reflections were used to solve the structure. Based on these data and 107 refined parameters R1=0.0359 (all data) wR2=0.0881 GOF (F2)=1.091. CCDC‐193487–193491 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre 12 Union Road Cambridge CB2 1EZ UK; fax: (+44) 1223‐336‐033; or deposit@ccdc.cam.ac.uk).
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Dates
Type When
Created 22 years, 6 months ago (Feb. 5, 2003, 8:54 p.m.)
Deposited 1 year, 10 months ago (Oct. 11, 2023, 3:16 p.m.)
Indexed 1 year, 1 month ago (July 23, 2024, 1:12 p.m.)
Issued 22 years, 6 months ago (Jan. 30, 2003)
Published 22 years, 6 months ago (Jan. 30, 2003)
Published Online 22 years, 6 months ago (Jan. 30, 2003)
Published Print 22 years, 6 months ago (Feb. 3, 2003)
Funders 0

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@article{Ren_2003, title={Nanoporous Lanthanide–Copper(<scp>II</scp>) Coordination Polymers: Syntheses and Crystal Structures of [{M2(Cu3(iminodiacetate)6)}⋅8 H2O]n (M=La, Nd, Eu)}, volume={42}, ISSN={1521-3773}, url={http://dx.doi.org/10.1002/anie.200390153}, DOI={10.1002/anie.200390153}, number={5}, journal={Angewandte Chemie International Edition}, publisher={Wiley}, author={Ren, Yan‐Ping and Long, La‐Sheng and Mao, Bing‐Wei and Yuan, You‐Zhu and Huang, Rong‐Bin and Zheng, Lan‐Sun}, year={2003}, month=jan, pages={532–535} }