DOI: 10.1002/anie.199502071. Mutually Interpenetrating Sheets and Channels in the Extended Structure of [Cu(4,4′‐bpy)Cl]

Mutually Interpenetrating Sheets and Channels in the Extended Structure of [Cu(4,4′‐bpy)Cl]

10.1002/anie.199502071

Crossref journal-article

Wiley

Angewandte Chemie International Edition in English (311)

Bibliography

Yaghi, O. M., & Li, G. (1995). Mutually Interpenetrating Sheets and Channels in the Extended Structure of [Cu(4,4â²âbpy)Cl]. Angewandte Chemie International Edition in English, 34(2), 207â209. Portico.

Authors 2

O. M. Yaghi (first)
Guangming Li (additional)

References 22 Referenced 303

{'key': 'e_1_2_1_1_2', 'series-title': 'Supramolecular Architecture: Synthetic Control in Thin Films and Solids', 'volume-title': 'ACS Symp. Ser.', 'author': 'Bein T.', 'year': '1992'} / ACS Symp. Ser. / Supramolecular Architecture: Synthetic Control in Thin Films and Solids by Bein T. (1992)
10.1021/ed067p829
10.1021/ja00081a067
10.1002/ange.19931050633
10.1002/anie.199308841
(b)T.Kitazawa H.Sugisawa M.Takeda T.Iwamoto J. Chem. Soc. Chem. Commun.1993 1855–1856. (10.1039/c39930001855)
10.1093/oso/9780198552932.003.0006 / Inclusion Compounds by Iwamoto T. (1991)
(d)R.Robson B. F.Abrahams S. R.Batten R. W.Gable B. F.Hoskins J.Liuin ref. [1a] p. 256.
10.1002/ange.19931050132
10.1002/anie.199300821
10.1021/ja00082a055
Elemental analysis: C10H8N2CuCl: calcd.: C 47.06 H 3.16 N 10.98 Cu 24.90 Cl 13.89; found.: C 47.34 H 3.03 N 11.11 Cu 25.84 Cl 13.00.
The homogeniety of the bulk product was confirmed by comparison of the observed and calculated X‐ray powder diffraction patterns. The calculated pattern was produced by using the SHELXTL‐XPOW program with the single‐crystal data.
Single crystals of [Cu(4 4′‐bpy)Cl] were analyzed at 20 °C. Tetragonal space groupI41/acd (no. 142) witha= 14.246(4) c= 38.596(12) Å V= 7833(3) Å3 Z= 16 ρcalcd= 1.731 gcm−3and μa(Mokα) = 2.46 mm−1. A total of 1345 independent absorption‐corrected reflections having 2θ(Mokα) < 45.8° (the equivalent of 0.6 Cukαspheres) were collected on a computer‐controlled Nicolet autodiffractometer with full 2.00° wide ω scans and graphite‐monochromated Mokαradiation. The structure was solved by direct methods (SHELXTLPC) and the resulting structural parameters were refined by least‐squares techniques to converge (R1 (unweighted based on |F|) = 0.050 for 465 independent absorption‐correction reflections having 2θ < 45.8° andI> 2σ(I)) using counter‐weighted full‐matrix least‐square techniques and a structural model which incorporated anisotropic thermal parameters for C8 C9 and C10 and for all hydrogen atoms. The hydrogen atoms were fixed at idealized sp2‐hybridized positions with CH bond lengths of 0.96 Å and their isotropic thermal parameters were fixed at values 1.2 times the equivalent isotropic thermal parameters of the carbon atoms to which they are covalently bonded. Further details on the crystal structure investigation may be obtained from the Fachinformationszentrum Karlsruhe D‐76344 Eggenstein‐Leopoldshafen (Germany) on quoting the depository number CSD‐58460.
10.1021/ar00178a001
{'key': 'e_1_2_1_9_3', 'volume-title': 'Catenanes, Rotaxanes, and Knots', 'author': 'Schill G.', 'year': '1988'} / Catenanes, Rotaxanes, and Knots by Schill G. (1988)
10.1002/ange.19931051032
10.1002/anie.199314951
(d)S. R.Batten B. F.Hoskins R.Robson J. Chem. Soc. Chem. Commun.1991 445–447. (10.1039/c39910000445)
(e)R. W.Gable B. F.Hoskins R.Robson J. Chem. Soc. Chem. Commun.1990 1677–1678. (10.1039/C39900001677)
10.1016/0022-1902(68)80444-0
{'key': 'e_1_2_1_11_2', 'first-page': '840', 'volume': '146', 'author': 'Gabuda S. P.', 'year': '1962', 'journal-title': 'Dokl. Akad. Nauk SSSR'} / Dokl. Akad. Nauk SSSR by Gabuda S. P. (1962)

Dates

Type	When
Created	21 years, 7 months ago (Jan. 16, 2004, 9:17 a.m.)
Deposited	1 year, 7 months ago (Jan. 11, 2024, 6:21 p.m.)
Indexed	3 days, 15 hours ago (Sept. 3, 2025, 5:53 a.m.)
Issued	30 years, 7 months ago (Feb. 3, 1995)
Published	30 years, 7 months ago (Feb. 3, 1995)
Published Online	21 years, 8 months ago (Dec. 22, 2003)
Published Print	30 years, 7 months ago (Feb. 3, 1995)

Funders 0

None

BibTeX

@article{Yaghi_1995, title={Mutually Interpenetrating Sheets and Channels in the Extended Structure of [Cu(4,4′‐bpy)Cl]}, volume={34}, ISSN={0570-0833}, url={http://dx.doi.org/10.1002/anie.199502071}, DOI={10.1002/anie.199502071}, number={2}, journal={Angewandte Chemie International Edition in English}, publisher={Wiley}, author={Yaghi, O. M. and Li, Guangming}, year={1995}, month=feb, pages={207–209} }

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