DOI: 10.1002/anie.199202301. Spontaneous Self‐Assembly of a Dinickel(<scp>II</scp>) Double Helicate Containing a 1, 3‐Benzenediyl Spacer Group

Spontaneous Self‐Assembly of a Dinickel(II) Double Helicate Containing a 1, 3‐Benzenediyl Spacer Group

10.1002/anie.199202301

Crossref journal-article

Wiley

Angewandte Chemie International Edition in English (311)

Bibliography

Constable, E. C., Hannon, M. J., & Tocher, D. A. (1992). Spontaneous SelfâAssembly of a Dinickel(II) Double Helicate Containing a 1, 3âBenzenediyl Spacer Group. Angewandte Chemie International Edition in English, 31(2), 230â232. Portico.

Authors 3

Edwin C. Constable (first)
Michael J. Hannon (additional)
Derek A. Tocher (additional)

References 53 Referenced 28

10.1002/ange.19911031107
{'key': 'e_1_2_1_1_3', 'first-page': '1451', 'volume': '30', 'year': '1991', 'journal-title': 'Angew. Chem. Int. Ed. Engl.'} / Angew. Chem. Int. Ed. Engl. (1991)
10.1038/346314a0
A full review of this topic is shortly to be published (E. C.Constable Tetrahedron in press).
10.1021/ic00203a021
10.1002/ange.19891011226
10.1002/anie.198916981
10.1039/j39660000098
10.1039/c39800000005
10.1107/S0567740881002665
10.1039/c39750000074
10.1021/ic50158a002
10.1039/dt9850001771
10.1021/ja00417a067
10.1021/ic00314a010
10.1021/ar00178a001
10.1002/ange.19901021034
10.1002/anie.199011541
10.1002/ange.19891010214
10.1002/anie.198901891
10.1021/ic00006a010
T. M.Garrett U.Koert J.‐M.Lehn A.Rigault D.Meyer J.Fischer J. Chem. Soc. Chem. Commun.1990 557; (10.1039/c39900000557)
{'key': 'e_1_2_1_3_3', 'first-page': '661', 'volume': '8', 'author': 'Gisselbrecht J.‐P.', 'year': '1984', 'journal-title': 'Nouv. J. Chim.'} / Nouv. J. Chim. by Gisselbrecht J.‐P. (1984)
10.1002/hlca.19910740317
10.1038/346339a0
{'key': 'e_1_2_1_3_6', 'first-page': '413', 'volume': '7', 'author': 'Lehn J.‐M.', 'year': '1983', 'journal-title': 'Nouv. J. Chim.'} / Nouv. J. Chim. by Lehn J.‐M. (1983)
10.1073/pnas.84.9.2565
10.1002/ange.19881000110
10.1002/anie.198800891
10.1002/ange.19881000824
10.1002/anie.198810951
10.1021/ic00009a035
M.Barley E. C.Constable S. A.Corr R. C. S.McQueen M. D.Ward M. G. B.Drew J. Chem. Soc. Dalton Trans.1988 2655;
10.1016/S0020-1693(00)84433-3
10.1039/C39870001600
10.1039/C39880001450
10.1016/S0277-5387(00)81155-9
10.1021/ja00167a093
10.1021/ja00159a062
10.1016/S0277-5387(00)81274-7
10.1039/dt9910001675
10.1016/S0277-5387(00)83560-3
1a:1H NMR (CD3SOCD3): δ =8.74 (br d; H6′) 7.51 (ddd; H5′) 8.02 (td; H4′) 8.66 (dd; H3′) 8.22 (dd; H3/5) 8.10 (t; H4) 8.41 (dd; H5/3) 9.07 (t;oH) 8.35 (dd;oH′) 7.72 (t;mH′); FAB‐MS (3‐nitrobenzylalcohol matrix):m/z387 307 289; EI‐MS:m/z386 308 231 159.1b:1H NMR (CD3SOCD3): δ =8.74 (br d; H6′) 7.51 (ddd; H5′) 8.01 (td; H4′) 8.65 (dd; H3′) 8.01 (d; H 3/5) 3.23 (s; SMe) 8.23 (d; H 5/3) 9.04 (t;oH′) 8.35 (dd; oH′) 7.70 (t;mH); FAB‐MS (3‐nitrobenzylalcohol matrix):m/z479; EI‐MS:m/z478 464 433 418. Coupling constants [Hz]:4J(o‐H o‐H′) 1.6 3J(o‐H′ m‐H) 7.8 3J(H4 H5) 7.7 4J(H3 H5) 1.5 4J(H3′/H4′) 7.9 3J(H3′ H5′) 1.5 3J(H4′ H5′) 7.7 3J(H5′ H6′) 4.8.
F.Kröhnke Synthesis1976 1.
{'key': 'e_1_2_1_7_2', 'first-page': '189', 'volume': '64', 'author': 'Potts K. T.', 'year': '1985', 'journal-title': 'Org. Synth.'} / Org. Synth. by Potts K. T. (1985)
10.1021/jo00137a001
10.1021/jo00015a050
10.1002/bscb.19900990911
10.1021/ja00247a021
[Cu2(1a)2](PF6)2:1H NMR (CD3CN): δ =7.65 (br d; H6′) 6.98 (dd; H5′) 7.80 (t; H4′) 7.98 (br d; H3′) 7.55 (d; H3/5) 7.95 (H4) 7.95 (H5/3) 9.6 (s;oH) 7.4 (d;oH′) 7.10 (t;mH). FAB‐MS (3‐nitrobenzylalcohol matrix):m/z449 [Cu(1a)] 835 [Cu(1a)2] 900 [Cu2(1a)2] 1046 [Cu2(1a)2(PF6)].
[Ag2(1a)2](PF6)2:1H NMR(CD3CN): δ =7.65 (v br d; H6′) 7.05 (ddd; H5′) 7.81 (t; H4′) 7.87 (br d; H3′) 7.48 (d H3/5) 7.95 (t H4) 7.88 (d; H5/3) 9.7 (s;oH) 7.52 (d;oH′) 7.28 (t;mH). FAB‐MS (3‐nitrobenyzlalcohol matrix):m/z495 [Ag(1a)] 880 [Ag(1a)2] 989 [Ag2(1a)2] 1133 [Ag2(1a)2(PF6)].
Crystal data for2: C60H50F12N8Ni2O4P2S4 monoclinic C2/c a=16.157(5) b=23.640(7) c=18.806(3) Å β =97.66(2)° V=7119(3) Å3 Mr=1482.7 Z=4 ϱber=1.38 gem−1 F(000) =3024 Moκαradiation λ =0.71073 Å μ(Moκα) =0.763 mm−1. The structure was solved by direct methods and refined by alternating cycles of least squares refinement and difference‐Fourier synthesis. All non‐hydrogen atoms anisotropic: H‐atoms riding on appropriate carbon atom with fixed isotropicU. 6611 reflections measured (5 < 2θ < 50°) corrected for absorption 3616 unique observed reflections withI> 6σ(I) R=0.0773 Rw=0.0793. Further details of the crystal structure investigation may be obtained from the Director of the Cambridge Crystallographic Data Centre University Chemical Laboratory Lensfield Road Cambridge CB2 1 EW (UK). Any request should be accompanied by the full literature citation for this communication.
10.1016/S0898-8838(08)60014-8

Dates

Type	When
Created	21 years, 8 months ago (Dec. 30, 2003, 6:08 p.m.)
Deposited	1 year, 10 months ago (Oct. 23, 2023, 1:17 p.m.)
Indexed	1 year, 10 months ago (Oct. 28, 2023, 3:17 a.m.)
Issued	33 years, 7 months ago (Feb. 1, 1992)
Published	33 years, 7 months ago (Feb. 1, 1992)
Published Online	21 years, 8 months ago (Dec. 22, 2003)
Published Print	33 years, 7 months ago (Feb. 1, 1992)

Funders 0

None

BibTeX

@article{Constable_1992, title={Spontaneous Self‐Assembly of a Dinickel(<scp>II</scp>) Double Helicate Containing a 1, 3‐Benzenediyl Spacer Group}, volume={31}, ISSN={0570-0833}, url={http://dx.doi.org/10.1002/anie.199202301}, DOI={10.1002/anie.199202301}, number={2}, journal={Angewandte Chemie International Edition in English}, publisher={Wiley}, author={Constable, Edwin C. and Hannon, Michael J. and Tocher, Derek A.}, year={1992}, month=feb, pages={230–232} }

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      "unstructured": "Crystal data for2: C60H50F12N8Ni2O4P2S4 monoclinic C2/c a=16.157(5) b=23.640(7) c=18.806(3) \u00c5 \u03b2 =97.66(2)\u00b0 V=7119(3) \u00c53 Mr=1482.7 Z=4 \u03f1ber=1.38 gem\u22121 F(000) =3024 Mo\u03ba\u03b1radiation \u03bb =0.71073 \u00c5 \u03bc(Mo\u03ba\u03b1) =0.763 mm\u22121. The structure was solved by direct methods and refined by alternating cycles of least squares refinement and difference\u2010Fourier synthesis. All non\u2010hydrogen atoms anisotropic: H\u2010atoms riding on appropriate carbon atom with fixed isotropicU. 6611 reflections measured (5 < 2\u03b8 < 50\u00b0) corrected for absorption 3616 unique observed reflections withI> 6\u03c3(I) R=0.0773 Rw=0.0793. Further details of the crystal structure investigation may be obtained from the Director of the Cambridge Crystallographic Data Centre University Chemical Laboratory Lensfield Road Cambridge CB2 1 EW (UK). Any request should be accompanied by the full literature citation for this communication."
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