DOI: 10.1002/ange.201104086. Actuation of Asymmetric Cyclopropanation Catalysts: Reversible Single‐Crystal to Single‐Crystal Reduction of Metal

Actuation of Asymmetric Cyclopropanation Catalysts: Reversible Single‐Crystal to Single‐Crystal Reduction of Metal–Organic Frameworks

10.1002/ange.201104086

Crossref journal-article

Wiley

Angewandte Chemie (311)

Bibliography

Falkowski, J. M., Wang, C., Liu, S., & Lin, W. (2011). Actuation of Asymmetric Cyclopropanation Catalysts: Reversible SingleâCrystal to SingleâCrystal Reduction of MetalâOrganic Frameworks. Angewandte Chemie, 123(37), 8833â8837. Portico.

Authors 4

Joseph M. Falkowski (first)
Cheng Wang (additional)
Sophie Liu (additional)
Wenbin Lin (additional)

References 66 Referenced 38

10.1002/ange.200801163
10.1002/anie.200801163
10.1002/ange.200462786
10.1002/anie.200462786
10.1002/ange.200461214
10.1002/anie.200461214
10.1021/ja1042935
10.1021/ja805235k
10.1002/ange.200805101
10.1002/anie.200805101
10.1021/ja106851d
10.1021/ja909629f
10.1016/j.cct.2003.08.004
10.1039/b807080f
10.1039/b807083k
10.1002/cite.201000188
10.1002/ange.200904958
10.1002/anie.200904958
10.1002/ange.200803387
10.1002/anie.200803387
10.1021/ja803383k
10.1038/nmat2608
10.1021/ja906198y
10.1002/ange.201003377
10.1002/anie.201003377
10.1021/ja0348344
10.1002/ange.200351264
10.1002/anie.200351264
10.1126/science.1083622
10.1021/ja973468j
10.1021/ja00163a052
10.1002/ange.200601918
10.1002/anie.200601918
10.1021/ja071046w
10.1002/ange.200704209
10.1002/anie.200704209
10.1002/ange.200352596
10.1002/anie.200352596
10.1021/ja710144k
10.1002/chem.200900037
10.1039/B600408C
10.1021/ja1069773
10.1039/c0cc05649a
10.1021/ja0466715
10.1071/CH06016
10.1002/ange.201004921
10.1002/anie.201004921
10.1002/ange.200907126
10.1002/anie.200907126
The determination of the unit cell and data collections for crystals of [Ru(L‐H2)(Py)2]Cl 1 1 R 2 and2 Rwere performed on a Bruker SMART APEX II diffractometer. Crystallographic data for [Ru(L‐H2)(Py)2]Cl: Monoclinic space groupC2 a=19.703(1) b=25.895(2) c=18.631(2) Å β=90.381(4)° V=9505.5(10) Å3 Z=8 ρcalcd=1.321 g cm−3 R1(I>2 σ(I))=0.0718 wR2(I>2 σ(I))=0.174. Crystallographic data for1: Trigonal space groupR32 a=29.750 (2) c=72.886(7) Å V=55 865(7) Å3 Z=6 ρcalcd=0.884 g cm−3 R1(I>2 σ(I))=0.177 wR2(I>2 σ(I))=0.401. Crystallographic data for2: Trigonal space groupR3 a=29.681 (1) c=72.690(2) Å V=55 457(2) Å3 Z=3 ρcalcd=0.445 g cm−3 R1(I>2 σ(I))=0.138 wR2(I>2 σ(I))=0.337. Crystallographic data for1 R: Trigonal space groupR32 a=29.798 (1) c=73.027(2) Å V=56 153(2) Å3 Z=6 ρcalcd=0.879 g cm−3 R1(I>2 σ(I))=0.163 wR2(I>2 σ(I))=0.376. Crystallographic data for2 R: Trigonal space groupR3 a=29.724 (1) c=72.861(2) Å V=55 750(2) Å3 Z=3 ρcalcd=0.443 g cm−3 R1(I>2 σ(I))=0.171 wR2(I>2 σ(I))=0.263. CCDC 816123 816124 816125 816126 and 816127 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre viawww.ccdc.cam.ac.uk/data_request/cif.
The solvent‐dependent catenation behavior observed here is different from the CMOFs built from manganese/salen struts (see Ref. [11b]) and probably a result of different solubility of the CMOFs in these solvents.
10.1038/nchem.738
10.1016/j.saa.2007.10.043
10.1002/1521-3757(20020816)114:16<3077::AID-ANGE3077>3.0.CO;2-O
10.1002/1521-3773(20020816)41:16<2953::AID-ANIE2953>3.0.CO;2-2
10.1126/science.1067208

Dates

Type	When
Created	14 years ago (Aug. 8, 2011, 9:25 a.m.)
Deposited	1 year, 10 months ago (Oct. 17, 2023, 6:08 p.m.)
Indexed	1 year, 1 month ago (July 8, 2024, 5:19 a.m.)
Issued	14 years ago (Aug. 8, 2011)
Published	14 years ago (Aug. 8, 2011)
Published Online	14 years ago (Aug. 8, 2011)
Published Print	13 years, 11 months ago (Sept. 5, 2011)

Funders 2

NSF
Awards1
1. CHE-0809776
DOE Office of Science
Awards1
1. DE-AC05-06OR23100

BibTeX

@article{Falkowski_2011, title={Actuation of Asymmetric Cyclopropanation Catalysts: Reversible Single‐Crystal to Single‐Crystal Reduction of Metal–Organic Frameworks}, volume={123}, ISSN={1521-3757}, url={http://dx.doi.org/10.1002/ange.201104086}, DOI={10.1002/ange.201104086}, number={37}, journal={Angewandte Chemie}, publisher={Wiley}, author={Falkowski, Joseph M. and Wang, Cheng and Liu, Sophie and Lin, Wenbin}, year={2011}, month=aug, pages={8833–8837} }

JSON

{
  "indexed": {
    "date-parts": [
      [
        2024,
        7,
        8
      ]
    ],
    "date-time": "2024-07-08T09:19:38Z",
    "timestamp": 1720430378782
  },
  "reference-count": 66,
  "publisher": "Wiley",
  "issue": "37",
  "license": [
    {
      "start": {
        "date-parts": [
          [
            2011,
            8,
            8
          ]
        ],
        "date-time": "2011-08-08T00:00:00Z",
        "timestamp": 1312761600000
      },
      "content-version": "vor",
      "delay-in-days": 0,
      "URL": "http://onlinelibrary.wiley.com/termsAndConditions#vor"
    }
  ],
  "funder": [
    {
      "name": "NSF",
      "award": [
        "CHE-0809776"
      ]
    },
    {
      "name": "DOE Office of Science",
      "award": [
        "DE-AC05-06OR23100"
      ]
    }
  ],
  "content-domain": {
    "domain": [],
    "crossmark-restriction": false
  },
  "published-print": {
    "date-parts": [
      [
        2011,
        9,
        5
      ]
    ]
  },
  "DOI": "10.1002/ange.201104086",
  "type": "journal-article",
  "created": {
    "date-parts": [
      [
        2011,
        8,
        8
      ]
    ],
    "date-time": "2011-08-08T13:25:13Z",
    "timestamp": 1312809913000
  },
  "page": "8833-8837",
  "source": "Crossref",
  "is-referenced-by-count": 38,
  "title": "Actuation of Asymmetric Cyclopropanation Catalysts: Reversible Single\u2010Crystal to Single\u2010Crystal Reduction of Metal\u2013Organic Frameworks",
  "prefix": "10.1002",
  "volume": "123",
  "author": [
    {
      "given": "Joseph M.",
      "family": "Falkowski",
      "sequence": "first",
      "affiliation": []
    },
    {
      "given": "Cheng",
      "family": "Wang",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "Sophie",
      "family": "Liu",
      "sequence": "additional",
      "affiliation": []
    },
    {
      "given": "Wenbin",
      "family": "Lin",
      "sequence": "additional",
      "affiliation": []
    }
  ],
  "member": "311",
  "published-online": {
    "date-parts": [
      [
        2011,
        8,
        8
      ]
    ]
  },
  "reference": [
    {
      "key": "e_1_2_3_1_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_2_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200801163"
    },
    {
      "key": "e_1_2_3_2_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200801163"
    },
    {
      "key": "e_1_2_3_3_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200462786"
    },
    {
      "key": "e_1_2_3_3_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200462786"
    },
    {
      "key": "e_1_2_3_4_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200461214"
    },
    {
      "key": "e_1_2_3_4_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200461214"
    },
    {
      "key": "e_1_2_3_5_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja1042935"
    },
    {
      "key": "e_1_2_3_6_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_7_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja805235k"
    },
    {
      "key": "e_1_2_3_8_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200805101"
    },
    {
      "key": "e_1_2_3_8_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200805101"
    },
    {
      "key": "e_1_2_3_9_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja106851d"
    },
    {
      "key": "e_1_2_3_10_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja909629f"
    },
    {
      "key": "e_1_2_3_11_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_12_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/j.cct.2003.08.004"
    },
    {
      "key": "e_1_2_3_13_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/b807080f"
    },
    {
      "key": "e_1_2_3_14_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/b807083k"
    },
    {
      "key": "e_1_2_3_15_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/cite.201000188"
    },
    {
      "key": "e_1_2_3_16_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_17_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200904958"
    },
    {
      "key": "e_1_2_3_17_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200904958"
    },
    {
      "key": "e_1_2_3_18_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200803387"
    },
    {
      "key": "e_1_2_3_18_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200803387"
    },
    {
      "key": "e_1_2_3_19_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_20_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja803383k"
    },
    {
      "key": "e_1_2_3_21_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1038/nmat2608"
    },
    {
      "key": "e_1_2_3_22_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja906198y"
    },
    {
      "key": "e_1_2_3_23_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.201003377"
    },
    {
      "key": "e_1_2_3_23_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.201003377"
    },
    {
      "key": "e_1_2_3_24_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_25_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja0348344"
    },
    {
      "key": "e_1_2_3_26_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200351264"
    },
    {
      "key": "e_1_2_3_26_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200351264"
    },
    {
      "key": "e_1_2_3_27_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_28_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1126/science.1083622"
    },
    {
      "key": "e_1_2_3_29_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja973468j"
    },
    {
      "key": "e_1_2_3_30_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja00163a052"
    },
    {
      "key": "e_1_2_3_31_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_32_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200601918"
    },
    {
      "key": "e_1_2_3_32_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200601918"
    },
    {
      "key": "e_1_2_3_33_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja071046w"
    },
    {
      "key": "e_1_2_3_34_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200704209"
    },
    {
      "key": "e_1_2_3_34_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200704209"
    },
    {
      "key": "e_1_2_3_35_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200352596"
    },
    {
      "key": "e_1_2_3_35_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200352596"
    },
    {
      "key": "e_1_2_3_36_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja710144k"
    },
    {
      "key": "e_1_2_3_37_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/chem.200900037"
    },
    {
      "key": "e_1_2_3_38_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_39_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/B600408C"
    },
    {
      "key": "e_1_2_3_40_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja1069773"
    },
    {
      "key": "e_1_2_3_40_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1039/c0cc05649a"
    },
    {
      "key": "e_1_2_3_41_2",
      "unstructured": "\u00a0"
    },
    {
      "key": "e_1_2_3_42_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1021/ja0466715"
    },
    {
      "key": "e_1_2_3_43_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1071/CH06016"
    },
    {
      "key": "e_1_2_3_44_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.201004921"
    },
    {
      "key": "e_1_2_3_44_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.201004921"
    },
    {
      "key": "e_1_2_3_45_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/ange.200907126"
    },
    {
      "key": "e_1_2_3_45_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/anie.200907126"
    },
    {
      "key": "e_1_2_3_46_2",
      "unstructured": "The determination of the unit cell and data collections for crystals of [Ru(L\u2010H2)(Py)2]Cl 1 1\u2009R 2 and2\u2009Rwere performed on a Bruker SMART APEX II diffractometer. Crystallographic data for [Ru(L\u2010H2)(Py)2]Cl: Monoclinic space groupC2 a=19.703(1) b=25.895(2) c=18.631(2)\u2005\u00c5 \u03b2=90.381(4)\u00b0 V=9505.5(10)\u2005\u00c53 Z=8 \u03c1calcd=1.321\u2005g\u2009cm\u22123 R1(I>2\u2009\u03c3(I))=0.0718 wR2(I>2\u2009\u03c3(I))=0.174. Crystallographic data for1: Trigonal space groupR32 a=29.750 (2) c=72.886(7)\u2005\u00c5 V=55\u2009865(7)\u2005\u00c53 Z=6 \u03c1calcd=0.884\u2005g\u2009cm\u22123 R1(I>2\u2009\u03c3(I))=0.177 wR2(I>2\u2009\u03c3(I))=0.401. Crystallographic data for2: Trigonal space groupR3 a=29.681 (1) c=72.690(2)\u2005\u00c5 V=55\u2009457(2)\u2005\u00c53 Z=3 \u03c1calcd=0.445\u2005g\u2009cm\u22123 R1(I>2\u2009\u03c3(I))=0.138 wR2(I>2\u2009\u03c3(I))=0.337. Crystallographic data for1\u2009R: Trigonal space groupR32 a=29.798 (1) c=73.027(2)\u2005\u00c5 V=56\u2009153(2)\u2005\u00c53 Z=6 \u03c1calcd=0.879\u2005g\u2009cm\u22123 R1(I>2\u2009\u03c3(I))=0.163 wR2(I>2\u2009\u03c3(I))=0.376. Crystallographic data for2\u2009R: Trigonal space groupR3 a=29.724 (1) c=72.861(2)\u2005\u00c5 V=55\u2009750(2)\u2005\u00c53 Z=3 \u03c1calcd=0.443\u2005g\u2009cm\u22123 R1(I>2\u2009\u03c3(I))=0.171 wR2(I>2\u2009\u03c3(I))=0.263. CCDC\u2005816123 816124 816125 816126 and 816127 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre viawww.ccdc.cam.ac.uk/data_request/cif."
    },
    {
      "key": "e_1_2_3_47_2",
      "unstructured": "The solvent\u2010dependent catenation behavior observed here is different from the CMOFs built from manganese/salen struts (see Ref.\u2005[11b]) and probably a result of different solubility of the CMOFs in these solvents."
    },
    {
      "key": "e_1_2_3_48_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1038/nchem.738"
    },
    {
      "key": "e_1_2_3_49_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1016/j.saa.2007.10.043"
    },
    {
      "key": "e_1_2_3_50_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/1521-3757(20020816)114:16<3077::AID-ANGE3077>3.0.CO;2-O"
    },
    {
      "key": "e_1_2_3_50_3",
      "doi-asserted-by": "publisher",
      "DOI": "10.1002/1521-3773(20020816)41:16<2953::AID-ANIE2953>3.0.CO;2-2"
    },
    {
      "key": "e_1_2_3_51_2",
      "doi-asserted-by": "publisher",
      "DOI": "10.1126/science.1067208"
    }
  ],
  "container-title": "Angewandte Chemie",
  "original-title": [],
  "language": "de",
  "link": [
    {
      "URL": "https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fange.201104086",
      "content-type": "application/pdf",
      "content-version": "vor",
      "intended-application": "text-mining"
    },
    {
      "URL": "https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2Fange.201104086",
      "content-type": "unspecified",
      "content-version": "vor",
      "intended-application": "text-mining"
    },
    {
      "URL": "https://onlinelibrary.wiley.com/doi/pdf/10.1002/ange.201104086",
      "content-type": "unspecified",
      "content-version": "vor",
      "intended-application": "similarity-checking"
    }
  ],
  "deposited": {
    "date-parts": [
      [
        2023,
        10,
        17
      ]
    ],
    "date-time": "2023-10-17T22:08:03Z",
    "timestamp": 1697580483000
  },
  "score": 1,
  "resource": {
    "primary": {
      "URL": "https://onlinelibrary.wiley.com/doi/10.1002/ange.201104086"
    }
  },
  "subtitle": [],
  "short-title": [],
  "issued": {
    "date-parts": [
      [
        2011,
        8,
        8
      ]
    ]
  },
  "references-count": 66,
  "journal-issue": {
    "issue": "37",
    "published-print": {
      "date-parts": [
        [
          2011,
          9,
          5
        ]
      ]
    }
  },
  "alternative-id": [
    "10.1002/ange.201104086"
  ],
  "URL": "http://dx.doi.org/10.1002/ange.201104086",
  "relation": {},
  "ISSN": [
    "0044-8249",
    "1521-3757"
  ],
  "subject": [],
  "container-title-short": "Angewandte Chemie",
  "published": {
    "date-parts": [
      [
        2011,
        8,
        8
      ]
    ]
  }
}