Crossref
journal-article
Wiley
Angewandte Chemie (311)
References
67
Referenced
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- Crystal data for1: C78H54Cl4Cu3Er7N9O37 Mr=3212.54 rhombohedral R$\bar 3$ a=18.2829(18) c=47.823(8) Å V=13 844(3) Å3 Z=6 ρ=2.312 g cm−3 μ=7.171 mm−1 F(000)=9072 GOF=1.153. A total of 35 759 reflections were collected and 7047 are unique (Rint=0.0717).R1/wR2=0.0587/0.1457 for 6808 reflections (I>2σ(I)) and 408 parameters.2: C78H54Br4Cu3Er7N9O37 Mr=3390.38 rhombohedral R$\bar 3$ a=18.3057(2) c=48.1567(3) Å V=13 975.3(2) Å3 Z=6 ρ=2.417 g cm−3 μ=8.705 mm−1 F(000)=9504 GOF=1.038. A total of 36 111 reflections were collected and 7121 are unique (Rint=0.0922).R1/wR2=0.0401/0.1044 for 415 parameters and 6184 reflections (I>2σ(I)). The intensity data were collected on a Mercury CCD diffractometer with graphite‐monochromated MoKαradiation (λ=0.71073 Å) at room temperature. All absorption corrections were performed by using the multiscan program. The structure were solved by direct methods and refined by full‐matrix least squares onF 2with the SHELXTL‐97 program.[20]All non‐hydrogen atoms except N2 disordered C11/C11′ and C12/C12′ in1and2 were refined anisotropically. CCDC‐279324 (1) and ‐279325 (2) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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- G. M. Sheldrick SHELXTL‐97 Program for the Solution of Crystal Structures University of Göttingen Germany 1997.
Dates
Type | When |
---|---|
Created | 19 years, 9 months ago (Nov. 28, 2005, 4:48 a.m.) |
Deposited | 1 year, 10 months ago (Oct. 17, 2023, 6:23 a.m.) |
Indexed | 1 year, 10 months ago (Oct. 18, 2023, 12:50 a.m.) |
Issued | 19 years, 8 months ago (Dec. 13, 2005) |
Published | 19 years, 8 months ago (Dec. 13, 2005) |
Published Online | 19 years, 8 months ago (Dec. 13, 2005) |
Published Print | 19 years, 8 months ago (Jan. 1, 2006) |
@article{Cheng_2005, title={Lanthanide–Transition‐Metal Sandwich Framework Comprising {Cu3} Cluster Pillars and Layered Networks of {Er36} Wheels}, volume={118}, ISSN={1521-3757}, url={http://dx.doi.org/10.1002/ange.200502917}, DOI={10.1002/ange.200502917}, number={1}, journal={Angewandte Chemie}, publisher={Wiley}, author={Cheng, Jian‐Wen and Zhang, Jie and Zheng, Shou‐Tian and Zhang, Man‐Bo and Yang, Guo‐Yu}, year={2005}, month=dec, pages={79–83} }