DOI: 10.1002/ange.200351718. Hochdurchsatz‐Hydrothermalsynthese anorganisch‐organischer Hybridverbindungen auf Basis von Phosphonaten

Hochdurchsatz‐Hydrothermalsynthese anorganisch‐organischer Hybridverbindungen auf Basis von Phosphonaten

10.1002/ange.200351718

Crossref journal-article

Wiley

Angewandte Chemie (311)

Bibliography

Stock, N., & Bein, T. (2004). HochdurchsatzâHydrothermalsynthese anorganischâorganischer Hybridverbindungen auf Basis von Phosphonaten. Angewandte Chemie, 116(6), 767â770. Portico.

Authors 2

Norbert Stock (first)
Thomas Bein (additional)

References 35 Referenced 47

10.1002/(SICI)1521-3757(19990201)111:3<335::AID-ANGE335>3.0.CO;2-U
10.1002/(SICI)1521-3773(19990201)38:3<323::AID-ANIE323>3.0.CO;2-4
10.1002/(SICI)1521-3757(19990215)111:4<507::AID-ANGE507>3.0.CO;2-I
10.1002/(SICI)1521-3773(19990215)38:4<483::AID-ANIE483>3.0.CO;2-#
10.1002/(SICI)1521-3757(19980302)110:5<629::AID-ANGE629>3.0.CO;2-4
10.1002/(SICI)1521-3773(19980316)37:5<609::AID-ANIE609>3.0.CO;2-X
10.1002/(SICI)1521-3757(19981217)110:24<3557::AID-ANGE3557>3.0.CO;2-7
10.1002/(SICI)1521-3773(19981231)37:24<3369::AID-ANIE3369>3.0.CO;2-H
10.1002/(SICI)1521-3757(19991004)111:19<3070::AID-ANGE3070>3.0.CO;2-9
10.1002/(SICI)1521-3773(19991004)38:19<2891::AID-ANIE2891>3.0.CO;2-X
10.1002/1521-3757(20010119)113:2<422::AID-ANGE422>3.0.CO;2-Z
10.1002/1521-3773(20010119)40:2<408::AID-ANIE408>3.0.CO;2-V
10.1039/b204496j
10.1016/S1293-2558(03)00157-2
10.1039/b006411o
10.1039/b006511k
10.1016/S1293-2558(02)01368-7
10.1016/S0022-4596(02)99537-X
10.1002/1521-3757(20020118)114:2<294::AID-ANGE294>3.0.CO;2-6
10.1002/1521-3773(20020118)41:2<284::AID-ANIE284>3.0.CO;2-M
10.1021/ar000034b
10.1039/b201381a
10.1002/1521-3757(20020118)114:2<291::AID-ANGE291>3.0.CO;2-I
10.1002/1521-3773(20020118)41:2<281::AID-ANIE281>3.0.CO;2-Y
10.1021/jo01343a067
10.1021/ic50145a047
CCDC‐208389 (1) ‐208390 (4) und ‐208391 (3) enthalten die ausführlichen kristallographischen Daten zu dieser Veröffentlichung. Die Daten sind kostenlos über www.ccdc.cam.ac.uk/conts/retrieving.html erhältlich (oder können bei folgender Adresse in Großbritannien angefordert werden: Cambridge Crystallographic Data Centre 12 Union Road Cambridge CB2 1EZ; Fax: (+44) 1223‐336‐033; oder deposit@ccdc.cam.ac.uk). Die Metalltetraphosphonate M(H6L1) sind unter folgenden Hinterlegungsnummern zu finden: CCDC‐206624 (M=Mn) CCDC‐208382 (M=Ca) CCDC‐208383 (M=Cd) CCDC‐208384 (M=Co) CCDC‐208385 (M=Fe) CCDC‐208386 (M=Mg) CCDC‐208387 (M=Ni) CCDC‐208388 (M=Zn).
Kristallographische Daten von1: Zn(HO3PCH2C6H4COOH)2 495.6 g mol−1 triklin P$\bar 1$ a=5.3512(2) b=11.3828(4) c=15.8307(5) Å α=99.338(2) β=92.850(2) γ=95.350(2)° V=945.28(6) Å3 Z=2 ρber.=1.741 g m−3 μ(MoKα)=1.523 mm−1 2θmax=27.52 19 481 gemessene Reflexe 4270 unabhängige Reflexe R1[I≥2σ(I)]=0.039 für 3242 Reflexe wR2=0.081 (Rint=0.066).
Da bisher nur sehr kleine plättchenförmige Kristalle erhalten werden konnten werden für2nur vorläufige kristallographische Daten angegeben: Zn(O3PCH2C6H4COOH) 279.48 g mol−1 triklin P$\bar 1$ a=5.1888(2) b=10.5838(5) c=17.3514(10) Å α=81.139(2) β=88.525(2) γ=89.389(3)° V=941.18(8) Å3 Z=4 ρber.=1.972 g m−3 μ(MoKα)=2.775 mm−1 2θmax=27.49 12 409 gemessene Reflexe 4235 unabhängige Reflexe R1[I≥2σ(I)]=0.1398 für 3174 Reflexe wR2=0.3875 (Rint=0.0834).
Kristallographische Daten von3: Zn3(O3PCH2C6H4COO)2⋅3 H2O 676.35 g mol−1 monoklin P21/a a=10.7950(2) b=9.3322(2) c=21.6181(4) β=91.584(1)° V=2177.0(1) Z=4 ρber.=2.064 g m−3 μ(MoKα)=3.494 mm−1 2θmax=27.49 28 743 gemessene Reflexe 4916 unabhängige Reflexe R1[I≥2σ(I)]=0.040 für 3040 Reflexe wR2=0.097 (Rint=0.097).
Kristallographische Daten von4: Zn(HO3PCH2C6H4COOH)2⋅4 H2O 567.66 g mol−1 triklin P$\bar 1$ a=4.7633(2) b=6.9325(4) c=16.5314(9) Å α=83.236(3) β=89.669(3) γ=83.006(2)° V=538.04(5) Å3 Z=1 ρber.=1.752 g m−3 μ(MoKα)=1.363 mm−1 2θmax=27.57 8881 gemessene Reflexe 2444 unabhängige Reflexe R1[I≥2σ(I)]=0.046 für 1708 Reflexe wR2=0.096 (Rint=0.0764).
N. Stock M. Rauscher T. Bein J. Solid State Chem. im Druck.
Stellvertretend für die sieben Metalltetraphosphonate M(H6L1) mit M=Mg Ca Fe Co Ni Cd oder Zn werden die kristallographischen Daten der Zinkverbindung angegeben: Zn(H6L1) 527.53 g mol−1 monoklin P21/a a=9.5077(2) b=9.0102(3) c=10.5520(3) Å β=104.7744(1)° V=874.10(4) Å3 Z=2 ρber.=2.004 g m−3 μ(MoKα)=1.838 mm−1 2θmax=27.43 9330 gemessene Reflexe 1982 unabhängige ReflexeR1[I≥2σ(I)]=0.039 für 1609 Reflexe wR2=0.093 (Rint=0.0584).
Accelerator Dual Dosing Station Chemspeed Ltd. Augst Schweiz.

Dates

Type	When
Created	21 years, 7 months ago (Jan. 27, 2004, 6:32 a.m.)
Deposited	1 year, 10 months ago (Oct. 11, 2023, 2:13 p.m.)
Indexed	2 months ago (June 27, 2025, 3:28 a.m.)
Issued	21 years, 7 months ago (Jan. 27, 2004)
Published	21 years, 7 months ago (Jan. 27, 2004)
Published Online	21 years, 7 months ago (Jan. 27, 2004)
Published Print	21 years, 7 months ago (Jan. 30, 2004)

Funders 0

None

BibTeX

@article{Stock_2004, title={Hochdurchsatz‐Hydrothermalsynthese anorganisch‐organischer Hybridverbindungen auf Basis von Phosphonaten}, volume={116}, ISSN={1521-3757}, url={http://dx.doi.org/10.1002/ange.200351718}, DOI={10.1002/ange.200351718}, number={6}, journal={Angewandte Chemie}, publisher={Wiley}, author={Stock, Norbert and Bein, Thomas}, year={2004}, month=jan, pages={767–770} }

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      "unstructured": "CCDC\u2010208389 (1) \u2010208390 (4) und \u2010208391 (3) enthalten die ausf\u00fchrlichen kristallographischen Daten zu dieser Ver\u00f6ffentlichung. Die Daten sind kostenlos \u00fcber www.ccdc.cam.ac.uk/conts/retrieving.html erh\u00e4ltlich (oder k\u00f6nnen bei folgender Adresse in Gro\u00dfbritannien angefordert werden: Cambridge Crystallographic Data Centre 12 Union Road Cambridge CB2\u20091EZ; Fax: (+44)\u20091223\u2010336\u2010033; oder deposit@ccdc.cam.ac.uk). Die Metalltetraphosphonate M(H6L1) sind unter folgenden Hinterlegungsnummern zu finden: CCDC\u2010206624 (M=Mn) CCDC\u2010208382 (M=Ca) CCDC\u2010208383 (M=Cd) CCDC\u2010208384 (M=Co) CCDC\u2010208385 (M=Fe) CCDC\u2010208386 (M=Mg) CCDC\u2010208387 (M=Ni) CCDC\u2010208388 (M=Zn)."
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      "unstructured": "Kristallographische Daten von1: Zn(HO3PCH2C6H4COOH)2 495.6 g\u2009mol\u22121 triklin P$\\bar 1$ a=5.3512(2) b=11.3828(4) c=15.8307(5) \u00c5 \u03b1=99.338(2) \u03b2=92.850(2) \u03b3=95.350(2)\u00b0 V=945.28(6) \u00c53 Z=2 \u03c1ber.=1.741 g\u2009m\u22123 \u03bc(MoK\u03b1)=1.523 mm\u22121 2\u03b8max=27.52 19\u2009481 gemessene Reflexe 4270 unabh\u00e4ngige Reflexe R1[I\u22652\u03c3(I)]=0.039 f\u00fcr 3242 Reflexe wR2=0.081 (Rint=0.066)."
    },
    {
      "key": "e_1_2_3_21_2",
      "unstructured": "Da bisher nur sehr kleine pl\u00e4ttchenf\u00f6rmige Kristalle erhalten werden konnten werden f\u00fcr2nur vorl\u00e4ufige kristallographische Daten angegeben: Zn(O3PCH2C6H4COOH) 279.48 g\u2009mol\u22121 triklin P$\\bar 1$ a=5.1888(2) b=10.5838(5) c=17.3514(10) \u00c5 \u03b1=81.139(2) \u03b2=88.525(2) \u03b3=89.389(3)\u00b0 V=941.18(8) \u00c53 Z=4 \u03c1ber.=1.972 g\u2009m\u22123 \u03bc(MoK\u03b1)=2.775 mm\u22121 2\u03b8max=27.49 12\u2009409 gemessene Reflexe 4235 unabh\u00e4ngige Reflexe R1[I\u22652\u03c3(I)]=0.1398 f\u00fcr 3174 Reflexe wR2=0.3875 (Rint=0.0834)."
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      "unstructured": "Kristallographische Daten von3: Zn3(O3PCH2C6H4COO)2\u22c53\u2009H2O 676.35 g\u2009mol\u22121 monoklin P21/a a=10.7950(2) b=9.3322(2) c=21.6181(4) \u03b2=91.584(1)\u00b0 V=2177.0(1) Z=4 \u03c1ber.=2.064 g\u2009m\u22123 \u03bc(MoK\u03b1)=3.494 mm\u22121 2\u03b8max=27.49 28\u2009743 gemessene Reflexe 4916 unabh\u00e4ngige Reflexe R1[I\u22652\u03c3(I)]=0.040 f\u00fcr 3040 Reflexe wR2=0.097 (Rint=0.097)."
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      "unstructured": "Kristallographische Daten von4: Zn(HO3PCH2C6H4COOH)2\u22c54\u2009H2O 567.66 g\u2009mol\u22121 triklin P$\\bar 1$ a=4.7633(2) b=6.9325(4) c=16.5314(9) \u00c5 \u03b1=83.236(3) \u03b2=89.669(3) \u03b3=83.006(2)\u00b0 V=538.04(5) \u00c53 Z=1 \u03c1ber.=1.752 g\u2009m\u22123 \u03bc(MoK\u03b1)=1.363 mm\u22121 2\u03b8max=27.57 8881 gemessene Reflexe 2444 unabh\u00e4ngige Reflexe R1[I\u22652\u03c3(I)]=0.046 f\u00fcr 1708 Reflexe wR2=0.096 (Rint=0.0764)."
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      "unstructured": "Stellvertretend f\u00fcr die sieben Metalltetraphosphonate M(H6L1) mit M=Mg Ca Fe Co Ni Cd oder Zn werden die kristallographischen Daten der Zinkverbindung angegeben: Zn(H6L1) 527.53 g\u2009mol\u22121 monoklin P21/a a=9.5077(2) b=9.0102(3) c=10.5520(3) \u00c5 \u03b2=104.7744(1)\u00b0 V=874.10(4) \u00c53 Z=2 \u03c1ber.=2.004 g\u2009m\u22123 \u03bc(MoK\u03b1)=1.838 mm\u22121 2\u03b8max=27.43 9330 gemessene Reflexe 1982 unabh\u00e4ngige ReflexeR1[I\u22652\u03c3(I)]=0.039 f\u00fcr 1609 Reflexe wR2=0.093 (Rint=0.0584)."
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      "unstructured": "Accelerator Dual Dosing Station Chemspeed Ltd. Augst Schweiz."
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